BRL 53080

Base Information

Chemical Name:BRL 53080
CAS No.:144930-19-8
Molecular Formula:C₂₀H₂₂Cl₂N₂OS
Molecular Weight:409.379
Hs Code.:

Synonyms:BRL 53080

Suppliers and Price of BRL 53080

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of BRL 53080

Chemical Property:

Purity/Quality:

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Technology Process of BRL 53080

There total 7 articles about BRL 53080 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59311-67-0
2-(3-thienyl)ethylamine

: 144930-19-8
BRL 53080

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / 50percent aq. K₂CO₃ / CH₂Cl₂ / Ambient temperature

2: 90 percent / phosphorus pentachloride, POCl₃ / 4 h / 40 °C

3: methanol / Ambient temperature

4: sodium borohydride / 2 h / 0 °C

5: K₂CO₃ / CH₂Cl₂ / 3 h / 0 °C

With sodium tetrahydroborate; phosphorus pentachloride; potassium carbonate; trichlorophosphate; In methanol; dichloromethane;
DOI:10.1021/jm00112a042

Reference yield:

: 144930-24-5
7-Pyrrolidin-1-ylmethyl-4,5,6,7-tetrahydro-thieno[2,3-c]pyridine

: 6831-55-6
2-(3,4-dichlorophenyl)acetyl chloride

: 144930-19-8
BRL 53080

Guidance literature:: With potassium carbonate; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1021/jm00112a042

Reference yield:

: 13781-53-8
(thiophen-3-yl)acetonitrile

: 144930-19-8
BRL 53080

Guidance literature:: Multi-step reaction with 6 steps

1: borane-methyl sulfide complex / tetrahydrofuran / 60 °C

2: 100 percent / 50percent aq. K₂CO₃ / CH₂Cl₂ / Ambient temperature

3: 90 percent / phosphorus pentachloride, POCl₃ / 4 h / 40 °C

4: methanol / Ambient temperature

5: sodium borohydride / 2 h / 0 °C

6: K₂CO₃ / CH₂Cl₂ / 3 h / 0 °C

With sodium tetrahydroborate; dimethylsulfide borane complex; phosphorus pentachloride; potassium carbonate; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm00112a042