Ni(OAc)2(H₂O)(N'-(furan-2-ylmethylene)-2-(4-methoxyphenylamino)acetohydrazide)*H₂O

Base Information

• Chemical Name: Ni(OAc)2(H₂O)(N'-(furan-2-ylmethylene)-2-(4-methoxyphenylamino)acetohydrazide)*H₂O
• CAS No.: 1130231-15-0
• Molecular Formula: C₁₈H₂₃N₃NiO₈*H₂O
• Molecular Weight: 486.101
• Mol file: 1130231-15-0.mol

Synonyms:Ni(OAc)2(H₂O)(N'-(furan-2-ylmethylene)-2-(4-methoxyphenylamino)acetohydrazide)*H₂O

Chemical Property of Ni(OAc)2(H₂O)(N'-(furan-2-ylmethylene)-2-(4-methoxyphenylamino)acetohydrazide)*H₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ni(OAc)2(H₂O)(N'-(furan-2-ylmethylene)-2-(4-methoxyphenylamino)acetohydrazide)*H₂O

There total 1 articles about Ni(OAc)2(H₂O)(N'-(furan-2-ylmethylene)-2-(4-methoxyphenylamino)acetohydrazide)*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(4-methoxyphenylamino)-N'-(furan-2-yl-methylene)acetohydrazide (303083-30-9) + nickel diacetate (373-02-4,14998-37-9,33025-09-1,94044-50-5,98268-31-6) → Ni(OAc)2(H2O)(N'-(furan-2-ylmethylene)-2-(4-methoxyphenylamino)acetohydrazide)*H2O (1130231-15-0)

Guidance literature:

In ethanol; hot EtOH soln. of ligand added to Ni-salt, heated at 80°C for 3 hwith stirring; filtered, washed with EtOH, dried under vac. over CaCl2; elem. anal.;

DOI:10.1016/j.saa.2008.09.015

Reference yield:

Ni(OAc)2(H2O)(N'-(furan-2-ylmethylene)-2-(4-methoxyphenylamino)acetohydrazide)*H2O (1130231-15-0) → nickel(II) oxide (1313-99-1)

Guidance literature:

In neat (no solvent, solid phase); Ni-complex heated to 1000°C in air at 10°C/min;

DOI:10.1016/j.saa.2008.09.015

upstream raw materials:

2-(4-methoxyphenylamino)-N'-(furan-2-yl-methylene)acetohydrazide

nickel diacetate

Downstream raw materials:

nickel(II) oxide