Benzenemethanamine, α-methyl-4-(1-methylethyl)-, (αR)-

Base Information

• Chemical Name: Benzenemethanamine, α-methyl-4-(1-methylethyl)-, (αR)-
• CAS No.: 856762-66-8
• Molecular Formula: C₁₁H₁₇N
• Molecular Weight: 163.263
• Hs Code.: 2921499090
• Mol file: 856762-66-8.mol

Synonyms:Benzenemethanamine, α-methyl-4-(1-methylethyl)-, (αR)-

Chemical Property of Benzenemethanamine, α-methyl-4-(1-methylethyl)-, (αR)-

Chemical Property:

• Vapor Pressure: 0.0483mmHg at 25°C
• Boiling Point: 236.1ºC at 760 mmHg
• Flash Point: 101.5ºC
• PSA: 26.02000
• Density: 0.923g/cm3
• LogP: 3.53000

Purity/Quality:

96% ^*data from raw suppliers

(R)-1-(4-ISOPROPYLPHENYL)ETHANAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenemethanamine, α-methyl-4-(1-methylethyl)-, (αR)-

There total 13 articles about Benzenemethanamine, α-methyl-4-(1-methylethyl)-, (αR)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-(4-Isopropylphenyl)-ethylamine*mandelic acid salt (98405-01-7,98405-03-9,98571-15-4) → (+)-1-(4-Isopropylphenyl)-ethylamine (68285-22-3,73441-43-7,98056-99-6,98405-02-8,856762-66-8)

Guidance literature:

With sodium hydroxide;

DOI:10.1055/s-1985-31162

Reference yield: 92.0%

1-(4-Isopropylphenyl)-ethylamine*mandelic acid (98405-01-7,98405-03-9,98571-15-4) → (-)-1-(4-Isopropylphenyl)-ethylamine (68285-22-3,73441-43-7,98056-99-6,98405-02-8,856762-66-8)

Guidance literature:

With sodium hydroxide;

DOI:10.1055/s-1985-31162

Reference yield:

[(S)-1-(4-Isopropyl-phenyl)-ethyl]-carbamic acid benzyl ester (222737-11-3) → (S)-1-(4-isopropylphenyl)ethylamine (68285-22-3,856762-66-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; for 0.75h; under 760 Torr;

DOI:10.1021/jm980612i

upstream raw materials:

1-(4-(prop-1-en-2-yl)phenyl)ethan-1-one

4-isopropylacetophenone

1-(4-Isopropyl-phenyl)-ethylamine; compound with (E)-3-phenyl-acrylic acid

1-(4-Isopropylphenyl)-ethylamine*mandelic acid salt

Downstream raw materials:

1-(4-Isopropyl-phenyl)-ethylamine; compound with (E)-3-phenyl-acrylic acid

1-(4-Isopropyl-phenyl)-ethylamine; compound with (E)-3-phenyl-acrylic acid

Refernces

• 1、 -. "Process for producing optically active 3,3,3-Trifluoro-2-Hydroxy-2-Methylpropionic acid, and salt thereof". . . Retrieved 2008/06/13.
• 2、 Saigo, Kazuhiko,Kai, Mariko,Yonezawa, Noriyuki,Hasegawa, Masaki,Nohura, Hiroyuki. "Synthesis and Optical Resolution of 1-(4-Isopropylphenyl)-ethylamine". . p. 214 - 216. Retrieved 2007/10/02.