1-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-3-methoxy-2-(benzyloxy)benzene

Base Information

Chemical Name:1-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-3-methoxy-2-(benzyloxy)benzene
CAS No.:147624-59-7
Molecular Formula:C₂₉H₃₇NO₅
Molecular Weight:479.616
Hs Code.:

Synonyms:1-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-3-methoxy-2-(benzyloxy)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-3-methoxy-2-(benzyloxy)benzene

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Technology Process of 1-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-3-methoxy-2-(benzyloxy)benzene

There total 2 articles about 1-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-3-methoxy-2-(benzyloxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 645-36-3
2,2-diethoxy-ethanamine

: 147624-56-4
(benzyloxy)methyl-(2-benzyloxy-3-methoxy)phenyl ketone

: 147624-59-7
1-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-3-methoxy-2-(benzyloxy)benzene

Guidance literature:: With sodium cyanoborohydride; magnesium sulfate; In methanol; acetic acid; Heating;
DOI:10.1080/00397919308009802

Reference yield:

: 147624-58-6
1-(2-benzyloxy-3-methoxyphenyl)-2-(benzyloxy)ethanol

: 147624-59-7
1-(1-(N-(2,2-diethoxyethyl)amino)-2-(benzyloxy)ethyl)-3-methoxy-2-(benzyloxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / NaOAc, PCC/Al₂O₃ / CH₂Cl₂ / Heating

2: 96 percent / NaCNBH₃, MgSO₄ / acetic acid; methanol / Heating

With aluminum oxide; sodium acetate; sodium cyanoborohydride; magnesium sulfate; pyridinium chlorochromate; In methanol; dichloromethane; acetic acid;
DOI:10.1080/00397919308009802