2-hydroxyethylamino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

Base Information

Chemical Name:2-hydroxyethylamino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione
CAS No.:313647-31-3
Molecular Formula:C₁₂H₁₄N₄O₂S₂
Molecular Weight:310.401
Hs Code.:

Synonyms:2-hydroxyethylamino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hydroxyethylamino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

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Technology Process of 2-hydroxyethylamino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

There total 2 articles about 2-hydroxyethylamino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1350301-74-4
5-(4-isothiocyanatophenyl)-2-methylsulfanyl-1,3,4-oxadiazole

: 141-43-5
ethanolamine

: 313647-31-3
2-hydroxyethylamino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

Guidance literature:: In benzene; for 3h; Reflux;
DOI:10.1016/j.bmc.2011.09.038

Reference yield:

: 5-(4-isothiocyanatophenyl)-1,3,4-oxadiazole-2-thiol

: 313647-31-3
2-hydroxyethylamino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / acetone / 2 h / 20 °C

2: benzene / 3 h / Reflux

With triethylamine; In acetone; benzene;
DOI:10.1016/j.bmc.2011.09.038