t-Butyl 3-(N-(3-(4,5-diethyl-1,6-dihydro-6-oxopyrimidin-2-yl)-4-n-propoxyphenyl) aminoformyl)propylaminoformate

Base Information

Chemical Name:t-Butyl 3-(N-(3-(4,5-diethyl-1,6-dihydro-6-oxopyrimidin-2-yl)-4-n-propoxyphenyl) aminoformyl)propylaminoformate
CAS No.:1229018-03-4
Molecular Formula:C₂₆H₃₈N₄O₅
Molecular Weight:486.612
Hs Code.:

Synonyms:t-Butyl 3-(N-(3-(4,5-diethyl-1,6-dihydro-6-oxopyrimidin-2-yl)-4-n-propoxyphenyl) aminoformyl)propylaminoformate

Suppliers and Price of t-Butyl 3-(N-(3-(4,5-diethyl-1,6-dihydro-6-oxopyrimidin-2-yl)-4-n-propoxyphenyl) aminoformyl)propylaminoformate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of t-Butyl 3-(N-(3-(4,5-diethyl-1,6-dihydro-6-oxopyrimidin-2-yl)-4-n-propoxyphenyl) aminoformyl)propylaminoformate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of t-Butyl 3-(N-(3-(4,5-diethyl-1,6-dihydro-6-oxopyrimidin-2-yl)-4-n-propoxyphenyl) aminoformyl)propylaminoformate

There total 2 articles about t-Butyl 3-(N-(3-(4,5-diethyl-1,6-dihydro-6-oxopyrimidin-2-yl)-4-n-propoxyphenyl) aminoformyl)propylaminoformate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 57294-38-9
N-(tert-butoxycarbonyl)-4-aminobutanoic acid

: 2-(5-amino-2-n-propoxyphenyl)-5,6-diethyl-4(3H)-pyrimidone hydrochloride

: 1229018-03-4
t-Butyl 3-(N-(3-(4,5-diethyl-1,6-dihydro-6-oxopyrimidin-2-yl)-4-n-propoxyphenyl) aminoformyl)propylaminoformate

Guidance literature:: N-(tert-butoxycarbonyl)-4-aminobutanoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 12h;

2-(5-amino-2-n-propoxyphenyl)-5,6-diethyl-4(3H)-pyrimidone hydrochloride; In dichloromethane; at 20 ℃; for 6h;

Reference yield:

: 1229017-38-2
2-(5-nitro-2-n-propoxyphenyl)-5,6-diethyl-4(3H)-pyrimidone

: 1229018-03-4
t-Butyl 3-(N-(3-(4,5-diethyl-1,6-dihydro-6-oxopyrimidin-2-yl)-4-n-propoxyphenyl) aminoformyl)propylaminoformate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogen / palladium 10% on activated carbon / methanol

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h / 20 °C

2.2: 6 h / 20 °C

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium 10% on activated carbon; In methanol; dichloromethane;