p-(N-(2-(2'-pyridyl))indolyl)phenyl-p-((9-(10-phenyl)anthracenyl)phenyl)dimethylsilane

Base Information

Chemical Name:p-(N-(2-(2'-pyridyl))indolyl)phenyl-p-((9-(10-phenyl)anthracenyl)phenyl)dimethylsilane
CAS No.:1404110-99-1
Molecular Formula:C₄₇H₃₆N₂Si
Molecular Weight:656.902
Hs Code.:

Synonyms:p-(N-(2-(2'-pyridyl))indolyl)phenyl-p-((9-(10-phenyl)anthracenyl)phenyl)dimethylsilane

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Chemical Property of p-(N-(2-(2'-pyridyl))indolyl)phenyl-p-((9-(10-phenyl)anthracenyl)phenyl)dimethylsilane

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Technology Process of p-(N-(2-(2'-pyridyl))indolyl)phenyl-p-((9-(10-phenyl)anthracenyl)phenyl)dimethylsilane

There total 3 articles about p-(N-(2-(2'-pyridyl))indolyl)phenyl-p-((9-(10-phenyl)anthracenyl)phenyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 13228-40-5
2-(2-pyridinyl)-1H-indole

: 1404110-96-8
p-iodophenyl-p-((9-(10-phenyl)anthracenyl)phenyl)dimethylsilane

: 1404110-99-1
p-(N-(2-(2'-pyridyl))indolyl)phenyl-p-((9-(10-phenyl)anthracenyl)phenyl)dimethylsilane

Guidance literature:: With copper(ll) sulfate pentahydrate; potassium carbonate; In dodecane; at 220 ℃; for 72h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol302742g

Reference yield:

: 23674-20-6
9-bromo-10-phenylanthracene

: 1404110-99-1
p-(N-(2-(2'-pyridyl))indolyl)phenyl-p-((9-(10-phenyl)anthracenyl)phenyl)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / -78 °C / Inert atmosphere

1.3: 48.5 h / 0 - 20 °C / Inert atmosphere

2.1: potassium carbonate; copper(ll) sulfate pentahydrate / dodecane / 72 h / 220 °C / Inert atmosphere; Schlenk technique

With n-butyllithium; copper(ll) sulfate pentahydrate; potassium carbonate; In tetrahydrofuran; dodecane; hexane; 1.1: |Negishi Coupling / 1.2: |Negishi Coupling / 1.3: |Negishi Coupling / 2.1: |Ullmann Condensation;
DOI:10.1021/ol302742g

Reference yield:

: 146748-21-2
bis(4-iodophenyl)dimethylsilane

: 1404110-99-1
p-(N-(2-(2'-pyridyl))indolyl)phenyl-p-((9-(10-phenyl)anthracenyl)phenyl)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / -78 °C / Inert atmosphere

1.3: 48.5 h / 0 - 20 °C / Inert atmosphere

2.1: potassium carbonate; copper(ll) sulfate pentahydrate / dodecane / 72 h / 220 °C / Inert atmosphere; Schlenk technique

With n-butyllithium; copper(ll) sulfate pentahydrate; potassium carbonate; In tetrahydrofuran; dodecane; hexane; 1.1: |Negishi Coupling / 1.2: |Negishi Coupling / 1.3: |Negishi Coupling / 2.1: |Ullmann Condensation;
DOI:10.1021/ol302742g