C₃₃H₃₈FN₅O₆S

Base Information

• Chemical Name: C₃₃H₃₈FN₅O₆S
• CAS No.: 868286-91-3
• Molecular Formula: C₃₃H₃₈FN₅O₆S
• Molecular Weight: 651.759
• Mol file: 868286-91-3.mol

Synonyms:C₃₃H₃₈FN₅O₆S

Chemical Property of C₃₃H₃₈FN₅O₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₃H₃₈FN₅O₆S

There total 11 articles about C₃₃H₃₈FN₅O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C33H40FN5O7S → C33H38FN5O6S (868286-91-3)

Guidance literature:

With sodium acetate; In ethanol; water; at 86 ℃; for 3h;

Reference yield:

tert-butyl [(1R)-2-amino-1-benzyl-2-(hydroxyimino)-1-methylethyl]carbamate (868286-29-7) → C33H38FN5O6S (868286-91-3)

Guidance literature:

Multi-step reaction with 2 steps

1: benzotriazol-1-ol; diisopropyl-carbodiimide / DMF (N,N-dimethyl-formamide); dichloromethane / 3 h / 20 °C

2: sodium acetate / ethanol; water / 3 h / 86 °C

With sodium acetate; benzotriazol-1-ol; diisopropyl-carbodiimide; In DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water;

Reference yield:

R-N-(tert-butoxycarbonyl)-α-methylphenylalaninamide (868286-30-0) → C33H38FN5O6S (868286-91-3)

Guidance literature:

Multi-step reaction with 4 steps

1: Burgess Reagent / 1,2-dichloro-ethane / 0.08 h / 100 °C / Microwave

2: hydroxylamine hydrochloride; water; potassium carbonate; isopropyl alcohol / 0.1 h / 130 °C / Microwave

3: benzotriazol-1-ol; diisopropyl-carbodiimide / DMF (N,N-dimethyl-formamide); dichloromethane / 3 h / 20 °C

4: sodium acetate / ethanol; water / 3 h / 86 °C

With Burgess Reagent; hydroxylamine hydrochloride; water; sodium acetate; potassium carbonate; benzotriazol-1-ol; isopropyl alcohol; diisopropyl-carbodiimide; In DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; 1,2-dichloro-ethane;

upstream raw materials:

R-N-(tert-butoxycarbonyl)-α-methylphenylalaninamide

tert-butyl [(1R)-2-amino-1-benzyl-2-(hydroxyimino)-1-methylethyl]carbamate

di-tert-butyl dicarbonate

(R)-2-amino-2-methyl-3-phenylpropanoic acid