12'-(4-methylthio-1-phenylpyrazolo[3,4-d]pyrimidin-6-ylthio)-N-ethyl-dodecanamide

Base Information

Chemical Name:12'-(4-methylthio-1-phenylpyrazolo[3,4-d]pyrimidin-6-ylthio)-N-ethyl-dodecanamide
CAS No.:188727-37-9
Molecular Formula:C₂₆H₃₇N₅OS₂
Molecular Weight:499.745
Hs Code.:

Synonyms:12'-(4-methylthio-1-phenylpyrazolo[3,4-d]pyrimidin-6-ylthio)-N-ethyl-dodecanamide

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Chemical Property of 12'-(4-methylthio-1-phenylpyrazolo[3,4-d]pyrimidin-6-ylthio)-N-ethyl-dodecanamide

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Technology Process of 12'-(4-methylthio-1-phenylpyrazolo[3,4-d]pyrimidin-6-ylthio)-N-ethyl-dodecanamide

There total 3 articles about 12'-(4-methylthio-1-phenylpyrazolo[3,4-d]pyrimidin-6-ylthio)-N-ethyl-dodecanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 188727-19-7
12'-(4-mercapto-1-phenylpyrazolo[3,4-d]pyrimidin-6-ylthio)-N-ethyl-dodecanamide

: 74-88-4
methyl iodide

: 188727-37-9
12'-(4-methylthio-1-phenylpyrazolo[3,4-d]pyrimidin-6-ylthio)-N-ethyl-dodecanamide

Guidance literature:: With sodium hydroxide; for 0.5h; Ambient temperature;
DOI:10.1016/S0968-0896(96)00240-4

Reference yield:

: 6289-02-7
1-phenyl-5H,7H-pyrazolo<3,4-d>pyrimidine-4,6-dithione

: 188727-37-9
12'-(4-methylthio-1-phenylpyrazolo[3,4-d]pyrimidin-6-ylthio)-N-ethyl-dodecanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / pyridine / 3 h / Ambient temperature

2: 60 percent / aq. 1.5 M NaOH / 0.5 h / Ambient temperature

With pyridine; sodium hydroxide;
DOI:10.1016/S0968-0896(96)00240-4

Reference yield:

: 12-Bromo-dodecanoic acid ethylamide

: 188727-37-9
12'-(4-methylthio-1-phenylpyrazolo[3,4-d]pyrimidin-6-ylthio)-N-ethyl-dodecanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / pyridine / 3 h / Ambient temperature

2: 60 percent / aq. 1.5 M NaOH / 0.5 h / Ambient temperature

With pyridine; sodium hydroxide;
DOI:10.1016/S0968-0896(96)00240-4