1-Phenyl-2,3-butadienyl tosylcarbamate

Base Information

• Chemical Name: 1-Phenyl-2,3-butadienyl tosylcarbamate
• CAS No.: 131141-51-0
• Molecular Formula: C₁₈H₁₇NO₄S
• Molecular Weight: 343.403

Synonyms:1-Phenyl-2,3-butadienyl tosylcarbamate

Chemical Property of 1-Phenyl-2,3-butadienyl tosylcarbamate

Chemical Property:

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Technology Process of 1-Phenyl-2,3-butadienyl tosylcarbamate

There total 2 articles about 1-Phenyl-2,3-butadienyl tosylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-phenylbuta-2,3-dien-1-ol (104516-09-8,124563-14-0,5732-13-8) + Tosyl isocyanate (4083-64-1) → 1-Phenyl-2,3-butadienyl tosylcarbamate (131141-51-0)

Guidance literature:

DOI:10.1016/S0040-4039(00)97592-0

Reference yield:

benzaldehyde (100-52-7) → 1-Phenyl-2,3-butadienyl tosylcarbamate (131141-51-0)

Guidance literature:

DOI:10.1016/S0040-4039(00)97592-0

Reference yield: 84.0%

1-Phenyl-2,3-butadienyl tosylcarbamate (131141-51-0) + acrolein (107-02-8,25068-14-8) → 4-[(4R,5R)-2-Oxo-5-phenyl-3-(toluene-4-sulfonyl)-oxazolidin-4-yl]-pent-4-enal

Guidance literature:

With palladium diacetate; lithium bromide; In tetrahydrofuran; at 20 ℃; for 5h;

DOI:10.1021/ol016727p

upstream raw materials:

1-phenylbuta-2,3-dien-1-ol

Tosyl isocyanate

benzaldehyde

Downstream raw materials:

(4S,5S)-4-(1-Iodo-vinyl)-5-phenyl-3-(toluene-4-sulfonyl)-oxazolidin-2-one

(4S,5R)-4-(1-Iodo-vinyl)-5-phenyl-3-(toluene-4-sulfonyl)-oxazolidin-2-one

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