1-phenyl-4-ethyl-1H-1,2,4-triazolium bis(trifluoromethylsulfonyl)imide

Base Information

• Chemical Name: 1-phenyl-4-ethyl-1H-1,2,4-triazolium bis(trifluoromethylsulfonyl)imide
• CAS No.: 1176199-58-8
• Molecular Formula: C₂F₆NO₄S₂*C₁₀H₁₂N₃
• Molecular Weight: 454.374

Synonyms:1-phenyl-4-ethyl-1H-1,2,4-triazolium bis(trifluoromethylsulfonyl)imide

Chemical Property of 1-phenyl-4-ethyl-1H-1,2,4-triazolium bis(trifluoromethylsulfonyl)imide

Chemical Property:

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Technology Process of 1-phenyl-4-ethyl-1H-1,2,4-triazolium bis(trifluoromethylsulfonyl)imide

There total 3 articles about 1-phenyl-4-ethyl-1H-1,2,4-triazolium bis(trifluoromethylsulfonyl)imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-ethyl-1-phenyl-1H-1,2,4-triazol-4-ium bromide (1176199-50-0) + bis(trifluoromethane)sulfonimide lithium (90076-65-6) → 1-phenyl-4-ethyl-1H-1,2,4-triazolium bis(trifluoromethylsulfonyl)imide (1176199-58-8)

Guidance literature:

In water;

DOI:10.1021/jo101784v

Reference yield:

iodobenzene (591-50-4) → 1-phenyl-4-ethyl-1H-1,2,4-triazolium bis(trifluoromethylsulfonyl)imide (1176199-58-8)

Guidance literature:

Multi-step reaction with 3 steps

1: copper(I) oxide; 1,10-Phenanthroline; potassium carbonate / N,N-dimethyl-formamide / 48 h / 120 °C / Inert atmosphere

2: 24 h / 110 °C / sealed tube

3: water

With copper(I) oxide; 1,10-Phenanthroline; potassium carbonate; In water; N,N-dimethyl-formamide;

DOI:10.1021/jo101784v

Reference yield:

1-phenyl-1H-1,2,4-triazole (13423-60-4) → 1-phenyl-4-ethyl-1H-1,2,4-triazolium bis(trifluoromethylsulfonyl)imide (1176199-58-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 24 h / 110 °C / sealed tube

2: water

In water;

DOI:10.1021/jo101784v

upstream raw materials:

1-phenyl-1H-1,2,4-triazole

4-ethyl-1-phenyl-1H-1,2,4-triazol-4-ium bromide

bis(trifluoromethane)sulfonimide lithium

iodobenzene

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