Z-Lys[3-carbamidopropyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-O-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranoside]-Gly-OBn

Base Information

Chemical Name:Z-Lys[3-carbamidopropyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-O-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranoside]-Gly-OBn
CAS No.:246516-50-7
Molecular Formula:C₅₃H₇₀N₄O₂₃
Molecular Weight:1131.15
Hs Code.:

Synonyms:Z-Lys[3-carbamidopropyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-O-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranoside]-Gly-OBn

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Z-Lys[3-carbamidopropyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-O-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranoside]-Gly-OBn

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Technology Process of Z-Lys[3-carbamidopropyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-O-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranoside]-Gly-OBn

There total 4 articles about Z-Lys[3-carbamidopropyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-O-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranoside]-Gly-OBn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.2%

: 1738-76-7
glycine benzyl ester p-toluenesulfonic acid salt

: 246516-49-4
Z-Lys[3-carbamidopropyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-O-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranoside]-OH

: 246516-50-7
Z-Lys[3-carbamidopropyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-O-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranoside]-Gly-OBn

Guidance literature:: With diphenyl-phosphinic acid; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 22h;
DOI:10.1021/jm000295r

Reference yield: 83.0%

: 1738-68-7
Gly-OBz

: 246516-49-4
Z-Lys[3-carbamidopropyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-O-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranoside]-OH

: 246516-50-7
Z-Lys[3-carbamidopropyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-O-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranoside]-Gly-OBn

Guidance literature:: With TEA; diphenyl-phosphinic acid; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1039/a904362d

Reference yield:

: 4-[(2R,3R,4R,5S,6R)-4-Acetoxy-6-acetoxymethyl-3-acetylamino-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-butyric acid 2,5-dioxo-pyrrolidin-1-yl ester

: 246516-50-7
Z-Lys[3-carbamidopropyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-O-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranoside]-Gly-OBn

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / dimethylformamide / 12 h / 20 °C

2: 83.2 percent / DPPA; Et₃N / dimethylformamide / 22 h / 20 °C

With diphenyl-phosphinic acid; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jm000295r