2-Chloro-4,6-dimethoxybenzaldehyde

Base Information

Chemical Name:2-Chloro-4,6-dimethoxybenzaldehyde
CAS No.:82477-61-0
Molecular Formula:C9H9ClO3
Molecular Weight:200.622
Hs Code.:2913000090
European Community (EC) Number:800-384-7
DSSTox Substance ID:DTXSID90397577
Wikidata:Q72518589
Mol file:82477-61-0.mol

Synonyms:2-Chloro-4,6-dimethoxybenzaldehyde;82477-61-0;2-Chloro-4,6-dimehoxybenzaldehyde;Benzaldehyde, 2-chloro-4,6-dimethoxy-;MFCD05863686;2-chloro-4,6-dimethoxy-benzaldehyde;SCHEMBL1428091;DTXSID90397577;WNIGZICIZZIUER-UHFFFAOYSA-N;AMY14389;6-Chloro-2,4-dimethoxy-benzaldehyde;BBL103653;STL557463;AKOS005257258;MS-20675;CS-0038443;FT-0600125;EN300-112791;F20278

Suppliers and Price of 2-Chloro-4,6-dimethoxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Chloro-4,6-dimethoxybenzaldehyde
100mg
$ 90.00

TRC
2-Chloro-4,6-dimethoxybenzaldehyde
500mg
$ 350.00

Crysdot
2-Chloro-4,6-dimethoxybenzaldehyde 95+%
5g
$ 831.00

American Custom Chemicals Corporation
2-CHLORO-4,6-DIMEHOXYBENZALDEHYDE 95.00%
1G
$ 867.12

Alichem
2-Chloro-4,6-dimethoxybenzaldehyde
1g
$ 263.94

AK Scientific
2-Chloro-4,6-dimethoxybenzaldehyde
1g
$ 600.80

Total 16 raw suppliers

Chemical Property of 2-Chloro-4,6-dimethoxybenzaldehyde

Chemical Property:

Vapor Pressure:0.000222mmHg at 25°C
Melting Point:79-80℃
Refractive Index:1.549
Boiling Point:326 °C at 760 mmHg
Flash Point:144.9 °C
PSA：35.53000
Density:1.245 g/cm³
LogP:2.16970
Storage Temp.:2-8°C
XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:200.0240218
Heavy Atom Count:13
Complexity:174

Purity/Quality:

97% ^*data from raw suppliers

2-Chloro-4,6-dimethoxybenzaldehyde ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C(=C1)Cl)C=O)OC

Technology Process of 2-Chloro-4,6-dimethoxybenzaldehyde

There total 5 articles about 2-Chloro-4,6-dimethoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.3%

: 7051-16-3
1-chloro-3,5-dimethoxybenzene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 82477-61-0
2-chloro-4,6-dimethoxybenzaldehyde

Guidance literature:: With trichlorophosphate; at 0 - 100 ℃; for 2.5h; Reflux;

Reference yield: 78.0%

: 7051-16-3
1-chloro-3,5-dimethoxybenzene

: 93-61-8
N-methyl-N-phenylformamide

: 82477-61-0
2-chloro-4,6-dimethoxybenzaldehyde

Guidance literature:: With trichlorophosphate; at 40 - 50 ℃;
DOI:10.1021/jm0493109

Reference yield:

: 637-62-7
p-benzoquinone oxime

: 82477-61-0
2-chloro-4,6-dimethoxybenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / hydrogen chloride gas / 25 - 30 °C

2: 92 percent / 1.) conc. hydrochloric acid, sodium nitrite, 2.) phosphinous acid / dioxane; H₂O / 20 h / 0 °C

3: 2.0 g / phosphoryl chloride / 0 deg C; room temperature, 0.5 h; 3 h

With hydrogenchloride; hypophosphorous acid; sodium nitrite; trichlorophosphate; In 1,4-dioxane; water;