C₂₃H₃₀N₂O₆S

Base Information

Chemical Name:C₂₃H₃₀N₂O₆S
CAS No.:78310-20-0
Molecular Formula:C₂₃H₃₀N₂O₆S
Molecular Weight:462.567
Hs Code.:

C<sub>23</sub>H<sub>30</sub>N<sub>2</sub>O<sub>6</sub>S

Synonyms:C₂₃H₃₀N₂O₆S

Suppliers and Price of C₂₃H₃₀N₂O₆S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of C₂₃H₃₀N₂O₆S

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of C₂₃H₃₀N₂O₆S

There total 2 articles about C₂₃H₃₀N₂O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 78310-19-7
4a-carbomethoxy-1,1-dimethyl-3,4,4a,5-tetrahydronaphthalene-2,6(1H,7H)-dione 6-ethylene acetal

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 78310-20-0
C₂₃H₃₀N₂O₆S

Guidance literature:: In methanol;
DOI:10.1021/ja00399a062

Reference yield: 80.0%

: 78310-19-7
4a-carbomethoxy-1,1-dimethyl-3,4,4a,5-tetrahydronaphthalene-2,6(1H,7H)-dione 6-ethylene acetal

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 78310-20-0
C₂₃H₃₀N₂O₆S

Guidance literature:: In methanol; at 55 ℃; for 15h;
DOI:10.1016/S0040-4020(01)90005-5

Reference yield:

: 78310-20-0
C₂₃H₃₀N₂O₆S

: 78310-36-8
3β,6,6-trimethyl-3α-hydroxy-2β-(2-hydroxy-4-methyl)phenyl-2α,2aβ,3,4,5,5aα,6,7,8,9,9a,10-dodecahydronaphthol<1,8a-c>furan

Guidance literature:: Multi-step reaction with 14 steps

1: 58 percent / NaB(CN)H₃, p-TsOH / tetrahydrothiophene 1,1-dioxide; dimethylformamide / 100 °C

2: 91 percent / LiAlH₄ / 1,2-dimethoxy-ethane

3: 97 percent / NaH / 1,2-dimethoxy-ethane

4: 100 percent / p-TsOH / acetone / 25 °C

5: 59 percent / p-TsOH / methanol / 50 °C

6: 1.) (i-Pr)2NLi / 1.) DME, -78 deg C

7: 100 percent / H₂ / Pd-C / ethanol

8: 89 percent / pyridinium tosylate / CH₂Cl₂

9: 99 percent / diethyl ether

10: 90 percent / PPTS, aq.EtOH / 60 °C

11: 80 percent / PCC / CH₂Cl₂

12: 1.) Li / 2.) DME, -75 -> 0 deg C

13: 78 percent / pyridinium chloride / CH₂Cl₂ / 0.5 h / 25 °C

14: 87 percent / NaSEt / dimethylformamide / 100 °C

With lithium aluminium tetrahydride; ethanol; hydrogen; pyridine hydrochloride; pyridinium p-toluenesulfonate; lithium; sodium hydride; sodium cyanoborohydride; toluene-4-sulfonic acid; pyridinium chlorochromate; lithium diisopropyl amide; sodium thioethylate; palladium on activated charcoal; In sulfolane; methanol; 1,2-dimethoxyethane; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ja00399a062