5-(2,3-di-O-acetyl-5-bromo-5-deoxy-β-D-ribofuranosyl)-3-benzyl-1-methyluracil

Base Information

Chemical Name:5-(2,3-di-O-acetyl-5-bromo-5-deoxy-β-D-ribofuranosyl)-3-benzyl-1-methyluracil
CAS No.:110419-27-7
Molecular Formula:C₂₁H₂₃BrN₂O₇
Molecular Weight:495.327
Hs Code.:

Synonyms:5-(2,3-di-O-acetyl-5-bromo-5-deoxy-β-D-ribofuranosyl)-3-benzyl-1-methyluracil

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Chemical Property of 5-(2,3-di-O-acetyl-5-bromo-5-deoxy-β-D-ribofuranosyl)-3-benzyl-1-methyluracil

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Technology Process of 5-(2,3-di-O-acetyl-5-bromo-5-deoxy-β-D-ribofuranosyl)-3-benzyl-1-methyluracil

There total 3 articles about 5-(2,3-di-O-acetyl-5-bromo-5-deoxy-β-D-ribofuranosyl)-3-benzyl-1-methyluracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 110419-26-6
5-(5-bromo-5-deoxy-β-D-ribofuranosyl)-3-benzyl-1-methyluracil

: 110419-27-7
5-(2,3-di-O-acetyl-5-bromo-5-deoxy-β-D-ribofuranosyl)-3-benzyl-1-methyluracil

Guidance literature:: With pyridine;
DOI:10.1021/jm00395a023

Reference yield:

: 100-39-0
benzyl bromide

: 110419-27-7
5-(2,3-di-O-acetyl-5-bromo-5-deoxy-β-D-ribofuranosyl)-3-benzyl-1-methyluracil

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Bu₂SnO / 1.) MeOH, reflux, 2.) DMF, a) RT, 3 h, b) 100 deg C, 1 h

2: 100 percent / pyridine

With pyridine; di(n-butyl)tin oxide;
DOI:10.1021/jm00395a023

Reference yield:

: 97416-19-8
4,5'-anhydro-1-methyl-5-(β-D-ribofuranosyl)uracil

: 110419-27-7
5-(2,3-di-O-acetyl-5-bromo-5-deoxy-β-D-ribofuranosyl)-3-benzyl-1-methyluracil

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Bu₂SnO / 1.) MeOH, reflux, 2.) DMF, a) RT, 3 h, b) 100 deg C, 1 h

2: 100 percent / pyridine

With pyridine; di(n-butyl)tin oxide;
DOI:10.1021/jm00395a023