(1S,2S,4S)-5-oxo-2-phenyl-bicyclo[2.2.1]heptane-2-carbonitrile ethylene ketal

Base Information

Chemical Name:(1S,2S,4S)-5-oxo-2-phenyl-bicyclo[2.2.1]heptane-2-carbonitrile ethylene ketal
CAS No.:1202008-33-0
Molecular Formula:C₁₆H₁₇NO₂
Molecular Weight:255.316
Hs Code.:

Synonyms:(1S,2S,4S)-5-oxo-2-phenyl-bicyclo[2.2.1]heptane-2-carbonitrile ethylene ketal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S,4S)-5-oxo-2-phenyl-bicyclo[2.2.1]heptane-2-carbonitrile ethylene ketal

Chemical Property:

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Technology Process of (1S,2S,4S)-5-oxo-2-phenyl-bicyclo[2.2.1]heptane-2-carbonitrile ethylene ketal

There total 3 articles about (1S,2S,4S)-5-oxo-2-phenyl-bicyclo[2.2.1]heptane-2-carbonitrile ethylene ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-oxo-2-phenyl-bicyclo[2.2.1]heptane-2-carbonitrile ethylene ketal

: 1202008-34-1
(1R,2S,4R)-5-oxo-2-phenyl-bicyclo[2.2.1]heptane-2-carbonitrile ethylene ketal

: 1202008-33-0
(1S,2S,4S)-5-oxo-2-phenyl-bicyclo[2.2.1]heptane-2-carbonitrile ethylene ketal

Guidance literature:: With Chiralpak AD-H; In methanol; n-heptane; isopropyl alcohol; Purification / work up; Resolution of racemate;

Reference yield:

: 1202008-32-9
5-oxo-bicyclo[2.2.1]heptane-2-carbonitrile ethylene ketal

: 1202008-33-0
(1S,2S,4S)-5-oxo-2-phenyl-bicyclo[2.2.1]heptane-2-carbonitrile ethylene ketal

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 20 h / 65 °C

2: Chiralpak AD-H / methanol; n-heptane; isopropyl alcohol / Resolution of racemate

With Chiralpak AD-H; In methanol; n-heptane; isopropyl alcohol; toluene;

Reference yield:

: 109459-54-3
2-keto cyclopentanone acetal

: 1202008-33-0
(1S,2S,4S)-5-oxo-2-phenyl-bicyclo[2.2.1]heptane-2-carbonitrile ethylene ketal

Guidance literature:: Multi-step reaction with 3 steps

1: hydroquinone / 1 h / 150 °C / Microwave irradiation

2: toluene / 20 h / 65 °C

3: Chiralpak AD-H / methanol; n-heptane; isopropyl alcohol / Resolution of racemate

With hydroquinone; In methanol; n-heptane; isopropyl alcohol; toluene;