methyl 2-((S)-1-(benzyloxy)-3-methylbutan-2-yl)-5-tert-butoxy-3-(2-methoxy-2-oxoethyl)isoxazolidine-3-carboxylate

Base Information

Chemical Name:methyl 2-((S)-1-(benzyloxy)-3-methylbutan-2-yl)-5-tert-butoxy-3-(2-methoxy-2-oxoethyl)isoxazolidine-3-carboxylate
CAS No.:1582763-27-6
Molecular Formula:C₂₄H₃₇NO₇
Molecular Weight:451.56
Hs Code.:

Synonyms:methyl 2-((S)-1-(benzyloxy)-3-methylbutan-2-yl)-5-tert-butoxy-3-(2-methoxy-2-oxoethyl)isoxazolidine-3-carboxylate

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Chemical Property of methyl 2-((S)-1-(benzyloxy)-3-methylbutan-2-yl)-5-tert-butoxy-3-(2-methoxy-2-oxoethyl)isoxazolidine-3-carboxylate

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Technology Process of methyl 2-((S)-1-(benzyloxy)-3-methylbutan-2-yl)-5-tert-butoxy-3-(2-methoxy-2-oxoethyl)isoxazolidine-3-carboxylate

There total 3 articles about methyl 2-((S)-1-(benzyloxy)-3-methylbutan-2-yl)-5-tert-butoxy-3-(2-methoxy-2-oxoethyl)isoxazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 926-02-3
tert-butyl vinyl ether

: 1582763-10-7
(S,E)-1-(benzyloxy)-N-(1,4-dimethoxy-1,4-dioxobutan-2-ylidene)-3-methylbutan-2-amine oxide

: 1582763-26-5
methyl 2-((S)-1-(benzyloxy)-3-methylbutan-2-yl)-5-tert-butoxy-3-(2-methoxy-2-oxoethyl)isoxazolidine-3-carboxylate

: methyl 2-((S)-1-(benzyloxy)-3-methylbutan-2-yl)-5-tert-butoxy-3-(2-methoxy-2-oxoethyl)isoxazolidine-3-carboxylate

: 1582763-27-6
methyl 2-((S)-1-(benzyloxy)-3-methylbutan-2-yl)-5-tert-butoxy-3-(2-methoxy-2-oxoethyl)isoxazolidine-3-carboxylate

Guidance literature:: at 80 ℃; for 312h; Overall yield = 83 %; Sealed tube;
DOI:10.1021/ol500483t

Reference yield:

: 537698-32-1
N-(1-benzyloxymethyl-2-methyl-propyl)-hydroxylamine

: 1582763-26-5
methyl 2-((S)-1-(benzyloxy)-3-methylbutan-2-yl)-5-tert-butoxy-3-(2-methoxy-2-oxoethyl)isoxazolidine-3-carboxylate

: methyl 2-((S)-1-(benzyloxy)-3-methylbutan-2-yl)-5-tert-butoxy-3-(2-methoxy-2-oxoethyl)isoxazolidine-3-carboxylate

: 1582763-27-6
methyl 2-((S)-1-(benzyloxy)-3-methylbutan-2-yl)-5-tert-butoxy-3-(2-methoxy-2-oxoethyl)isoxazolidine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 30 h / 0 - 20 °C

2: 312 h / 80 °C / Sealed tube

In dichloromethane;
DOI:10.1021/ol500483t

Reference yield:

: 762-42-5
dimethyl acetylenedicarboxylate

: 1582763-26-5
methyl 2-((S)-1-(benzyloxy)-3-methylbutan-2-yl)-5-tert-butoxy-3-(2-methoxy-2-oxoethyl)isoxazolidine-3-carboxylate

: methyl 2-((S)-1-(benzyloxy)-3-methylbutan-2-yl)-5-tert-butoxy-3-(2-methoxy-2-oxoethyl)isoxazolidine-3-carboxylate

: 1582763-27-6
methyl 2-((S)-1-(benzyloxy)-3-methylbutan-2-yl)-5-tert-butoxy-3-(2-methoxy-2-oxoethyl)isoxazolidine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 30 h / 0 - 20 °C

2: 312 h / 80 °C / Sealed tube

In dichloromethane;
DOI:10.1021/ol500483t