Technology Process of PYRIDINE-3-SULFONYL CHLORIDE HYDROCHLORIDE
There total 12 articles about PYRIDINE-3-SULFONYL CHLORIDE HYDROCHLORIDE which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
phosphorus pentachloride;
In
trichlorophosphate;
at 120 ℃;
for 12h;
DOI:10.1021/ja00038a065
- Guidance literature:
-
In
chlorobenzene;
at 85 ℃;
under 172.517 Torr;
- Guidance literature:
-
pyridin-3-ylamine;
With
hydrogenchloride; sodium nitrite;
In
water;
at -5 - 0 ℃;
Large scale;
Green chemistry;
With
thionyl chloride; sulphurous acid; copper(l) chloride;
In
water;
at 0 - 4 ℃;
for 1.5h;
Concentration;
Reagent/catalyst;
Large scale;
Green chemistry;
Xi
