2-(4-Benzyloxy-3-methoxy-phenyl)-5-oxo-tetrahydro-furan-3-carboxylic acid

Base Information

• Chemical Name: 2-(4-Benzyloxy-3-methoxy-phenyl)-5-oxo-tetrahydro-furan-3-carboxylic acid
• CAS No.: 86841-94-3
• Molecular Formula: C₁₉H₁₈O₆
• Molecular Weight: 342.348

Synonyms:2-(4-Benzyloxy-3-methoxy-phenyl)-5-oxo-tetrahydro-furan-3-carboxylic acid

Chemical Property of 2-(4-Benzyloxy-3-methoxy-phenyl)-5-oxo-tetrahydro-furan-3-carboxylic acid

Chemical Property:

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Technology Process of 2-(4-Benzyloxy-3-methoxy-phenyl)-5-oxo-tetrahydro-furan-3-carboxylic acid

There total 3 articles about 2-(4-Benzyloxy-3-methoxy-phenyl)-5-oxo-tetrahydro-furan-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

succinic acid anhydride (108-30-5) + 3-methoxy-4-(phenylmethoxy)benzaldehyde (2426-87-1) → 2-(4-Benzyloxy-3-methoxy-phenyl)-5-oxo-tetrahydro-furan-3-carboxylic acid (86841-94-3)

Guidance literature:

With triethylamine; zinc(II) chloride; In dichloromethane; for 24h;

DOI:10.1016/S0040-4039(00)81886-9

Reference yield:

succinic acid anhydride (108-30-5) + 3-methoxy-4-(phenylmethoxy)benzaldehyde (2426-87-1) → trans-(4-benzyloxy-3-methoxyphenyl)-4-carboxydihydrofuran-2(3H)-one (86841-94-3,139714-51-5,139714-52-6) + cis-(4-benzyloxy-3-methoxyphenyl)-4-carboxydihydrofuran-2(3H)-one (86841-94-3,139714-51-5,139714-52-6)

Guidance literature:

With triethylamine; zinc(II) chloride; In dichloromethane; Yield given. Yields of byproduct given;

Reference yield:

succinic acid anhydride (108-30-5) + 3-methoxy-4-(phenylmethoxy)benzaldehyde (2426-87-1) → trans-(4-benzyloxy-3-methoxyphenyl)-4-carboxydihydrofuran-2(3H)-one (86841-94-3,139714-51-5,139714-52-6) + cis-(4-benzyloxy-3-methoxyphenyl)-4-carboxydihydrofuran-2(3H)-one (86841-94-3,139714-51-5,139714-52-6)

Guidance literature:

With triethylamine; zinc(II) chloride; In dichloromethane; Yield given. Yields of byproduct given;

upstream raw materials:

succinic acid anhydride

3-methoxy-4-(phenylmethoxy)benzaldehyde

Downstream raw materials:

4-endo-8-exo-bis-(4-hydroxy-3-methoxyphenyl)-3,7-dioxabicyclo<3.3.0>octan-2-one

cis-5-(4-benzyloxy-3-methoxyphenyl)-4-hydroxymethyldihydrofuran-2(3H)-one

trans-5-(4-benzyloxy-3-methoxyphenyl)-4-hydroxymethyldihydrofuran-2(3H)-one

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