coniferyl alcohol 2,4-dinitrophenyl ether

Base Information

• Chemical Name: coniferyl alcohol 2,4-dinitrophenyl ether
• CAS No.: 67638-42-0
• Molecular Formula: C₁₆H₁₄N₂O₇
• Molecular Weight: 346.296
• Mol file: 67638-42-0.mol

Synonyms:coniferyl alcohol 2,4-dinitrophenyl ether

Chemical Property of coniferyl alcohol 2,4-dinitrophenyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of coniferyl alcohol 2,4-dinitrophenyl ether

There total 1 articles about coniferyl alcohol 2,4-dinitrophenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

coniferal alcohol (458-35-5,32811-40-8,69056-21-9) + 2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) → coniferyl alcohol 2,4-dinitrophenyl ether (67638-42-0)

Guidance literature:

Reference yield: 81.0%

coniferyl alcohol 2,4-dinitrophenyl ether (67638-42-0) + <9-(13)C>-p-coumaroyl chloride 2,4-dinitrophenyl ether → C30(13)CH22N4O13

Guidance literature:

With dmap; triethylamine; In dichloromethane; for 1h; Ambient temperature;

DOI:10.1021/ja00100a006

Reference yield:

coniferyl alcohol 2,4-dinitrophenyl ether (67638-42-0) → <9-13C>coniferyl p-coumarate

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / triethylamine, 4-(dimethylamino)pyridine / CH₂Cl₂ / 1 h / Ambient temperature

2: 80 percent / piperazine / benzene / Heating

With piperazine; dmap; triethylamine; In dichloromethane; benzene;

DOI:10.1021/ja00100a006

upstream raw materials:

coniferal alcohol

2,4-Dinitrofluorobenzene

Downstream raw materials:

(E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-[4-(2,4-dinitro-phenoxy)-3-methoxy-phenyl]-allyl ester

(E)-3-(4-Hydroxy-phenyl)-acrylic acid (E)-3-(4-hydroxy-3-methoxy-phenyl)-allyl ester