methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-galactopyranoside

Base Information

Chemical Name:methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-galactopyranoside
CAS No.:95239-49-9
Molecular Formula:C₂₁H₂₂FNO₅
Molecular Weight:387.408
Hs Code.:

Synonyms:methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-galactopyranoside

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Chemical Property of methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-galactopyranoside

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Technology Process of methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-galactopyranoside

There total 6 articles about methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 95239-47-7
methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-α-D-arabino-hex-5-enopyranoside

: 95239-49-9
methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-galactopyranoside

: 95239-46-6
methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-α-D-altropyranoside

Guidance literature:: With hydrogen; Kuhn catalyst; In methanol; for 2h; Ambient temperature;
DOI:10.1016/0008-6215(85)85123-5

Reference yield: 41.0%

: 95239-47-7
methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-α-D-arabino-hex-5-enopyranoside

: 95239-48-8
methyl 3-benzamido-2,3,4,6-tetradeoxy-2-fluoro-α-D-threo-hex-5-enopyranoside

: 95239-49-9
methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-galactopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 8h; Ambient temperature;
DOI:10.1016/0008-6215(84)85015-6

Reference yield:

: 74801-07-3
methyl 3-benzamido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-altropyranoside

: 95239-49-9
methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / barium carbonate, benzoyl peroxide, N-bromosuccinimide / CCl₄ / 3 h / Heating

2: 74 percent / 1,5-diazabicyclo<5.4.0>undec-5-ene / hexamethylphosphoric acid triamide / 96 h / Ambient temperature

3: 41 percent / H₂ / 5percent Pd/C / ethyl acetate / 8 h / Ambient temperature

With N-Bromosuccinimide; Perbenzoic acid; hydrogen; barium carbonate; 1,5-Diazabicyclo[5.4.0]undec-5-ene; palladium on activated charcoal; In tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide; ethyl acetate;
DOI:10.1016/0008-6215(84)85015-6