butyl 7β-(1-benzamido-3-oxo-trans-1-octenyl)-1,4-dioxaspiro<4.4>nonane-6α-heptanoate

Base Information

Chemical Name:butyl 7β-(1-benzamido-3-oxo-trans-1-octenyl)-1,4-dioxaspiro<4.4>nonane-6α-heptanoate
CAS No.:78200-04-1
Molecular Formula:C₃₃H₄₉NO₆
Molecular Weight:555.755
Hs Code.:

Synonyms:butyl 7β-(1-benzamido-3-oxo-trans-1-octenyl)-1,4-dioxaspiro<4.4>nonane-6α-heptanoate

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Chemical Property of butyl 7β-(1-benzamido-3-oxo-trans-1-octenyl)-1,4-dioxaspiro<4.4>nonane-6α-heptanoate

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Technology Process of butyl 7β-(1-benzamido-3-oxo-trans-1-octenyl)-1,4-dioxaspiro<4.4>nonane-6α-heptanoate

There total 7 articles about butyl 7β-(1-benzamido-3-oxo-trans-1-octenyl)-1,4-dioxaspiro<4.4>nonane-6α-heptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52477-97-1
2-(7-butoxycarbonylhexyl)-2-cyclopenten-1-one

: 78200-04-1
butyl 7β-(1-benzamido-3-oxo-trans-1-octenyl)-1,4-dioxaspiro<4.4>nonane-6α-heptanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 2) pyridinium p-toluenesulfonate / 1) tetramethylguanidine

2: 72 percent / PhNCO, NEt₃ / 1) room temperrature, overnight, 2) 50 deg C, 1 h

3: 66 percent / γ-MnO2

4: H₂ / PtO₂, Raney nickel / methanol

5: 1.4 g / pyridine / Ambient temperature

With pyridine; manganese(IV) oxide; hydrogen; pyridinium p-toluenesulfonate; phenyl isocyanate; triethylamine; platinum(IV) oxide; 1,1,3,3-tetramethylguanidine; nickel; In methanol;
DOI:10.1021/jo00335a040

Reference yield:

: 78199-98-1
butyl 7β-(nitromethyl)-1,4-dioxaspiro<4.4>nonane-6α-heptanoate

: 78200-04-1
butyl 7β-(1-benzamido-3-oxo-trans-1-octenyl)-1,4-dioxaspiro<4.4>nonane-6α-heptanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / PhNCO, NEt₃ / 1) room temperrature, overnight, 2) 50 deg C, 1 h

2: 66 percent / γ-MnO2

3: H₂ / PtO₂, Raney nickel / methanol

4: 1.4 g / pyridine / Ambient temperature

With pyridine; manganese(IV) oxide; hydrogen; phenyl isocyanate; triethylamine; platinum(IV) oxide; nickel; In methanol;
DOI:10.1021/jo00335a040

Reference yield:

: 592-76-7
1-Heptene

: 78200-04-1
butyl 7β-(1-benzamido-3-oxo-trans-1-octenyl)-1,4-dioxaspiro<4.4>nonane-6α-heptanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / PhNCO, NEt₃ / 1) room temperrature, overnight, 2) 50 deg C, 1 h

2: 66 percent / γ-MnO2

3: H₂ / PtO₂, Raney nickel / methanol

4: 1.4 g / pyridine / Ambient temperature

With pyridine; manganese(IV) oxide; hydrogen; phenyl isocyanate; triethylamine; platinum(IV) oxide; nickel; In methanol;
DOI:10.1021/jo00335a040