N-benzyloxycarbonyl-2,2-difluoro-1-ethylsulfonylethylamine

Base Information

Chemical Name:N-benzyloxycarbonyl-2,2-difluoro-1-ethylsulfonylethylamine
CAS No.:154140-60-0
Molecular Formula:C₁₂H₁₅F₂NO₄S
Molecular Weight:307.318
Hs Code.:

Synonyms:N-benzyloxycarbonyl-2,2-difluoro-1-ethylsulfonylethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyloxycarbonyl-2,2-difluoro-1-ethylsulfonylethylamine

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Technology Process of N-benzyloxycarbonyl-2,2-difluoro-1-ethylsulfonylethylamine

There total 2 articles about N-benzyloxycarbonyl-2,2-difluoro-1-ethylsulfonylethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 154140-59-7
N-benzyloxycarbonyl-2,2-difluoro-1-ethylthioethylamine

: 154140-60-0
N-benzyloxycarbonyl-2,2-difluoro-1-ethylsulfonylethylamine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile; 1.) -20 deg C, 105 min; 2.) 0 deg C, 1 h; 3.) RT, 16 h;
DOI:10.1055/s-1993-25979

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 154140-60-0
N-benzyloxycarbonyl-2,2-difluoro-1-ethylsulfonylethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / pyridine / CH₂Cl₂ / 1.) -10 deg C, 40 min; 2.) up to 0 deg C, 4 h; 3.) RT

2: 79 percent / MCPBA / CH₂Cl₂; acetonitrile / 1.) -20 deg C, 105 min; 2.) 0 deg C, 1 h; 3.) RT, 16 h

With pyridine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile;
DOI:10.1055/s-1993-25979