2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-3,4-dihydro-1(2H)-isoquinoline

Base Information

• Chemical Name: 2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-3,4-dihydro-1(2H)-isoquinoline
• CAS No.: 145160-04-9
• Molecular Formula: C₁₉H₂₁NO₄
• Molecular Weight: 327.38

Synonyms:2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-3,4-dihydro-1(2H)-isoquinoline

Chemical Property of 2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-3,4-dihydro-1(2H)-isoquinoline

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Technology Process of 2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-3,4-dihydro-1(2H)-isoquinoline

There total 7 articles about 2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-3,4-dihydro-1(2H)-isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

α-(3,4-dimethoxyphenyl)-3,4-dihydro-2(1H)-isoquinolineethanol (145160-03-8) → 2-(3,4-dimethoxyphenyl)-2,3,6,10b-tetrahydro-5H-oxazolo<2,3-a>isoquinoline (145160-05-0,145160-14-1) + 2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-3,4-dihydro-1(2H)-isoquinoline (145160-04-9)

Guidance literature:

With mercury(II) diacetate; edetate disodium; In sodium hydroxide; water; for 3h; Heating;

Reference yield: 57.0%

2-(3,4-dimethoxyphenyl)-2,3,6,10b-tetrahydro-5H-oxazolo<2,3-a>isoquinoline (145160-05-0,145160-14-1) → 2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-3,4-dihydro-1(2H)-isoquinoline (145160-04-9)

Guidance literature:

With mercury(II) diacetate; edetate disodium; In water; acetic acid; for 24h; Heating;

Reference yield: 38.0%

α-(3,4-dimethoxyphenyl)-3,4-dihydro-2(1H)-isoquinolineethanol (145160-03-8) → 2-(3,4-dimethoxyphenyl)-2,3,6,10b-tetrahydro-5H-oxazolo<2,3-a>isoquinoline (145160-05-0,145160-14-1) + 2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-1(2H)-isoquinoline (145160-06-1) + 2-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-3,4-dihydro-1(2H)-isoquinoline (145160-04-9)

Guidance literature:

With mercury(II) diacetate; edetate disodium; In water; acetic acid; at 110 ℃; for 1.5h;

upstream raw materials:

2-(3,4-dimethoxyphenyl)-2,3,6,10b-tetrahydro-5H-oxazolo<2,3-a>isoquinoline

α-(3,4-dimethoxyphenyl)-3,4-dihydro-2(1H)-isoquinolineethanol

1,2,3,4-tetrahydroisoquinoline

2-Bromo-1-(3,4-dimethoxyphenyl)ethanone

Downstream raw materials:

2-<2-(3,4-dimethoxyphenyl)ethyl>-3,4-dihydro-1(2H)-isoquinoline

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