1-{{1-{(2Z)-2-phenyl-2-[(phenylmethoxy)imino]ethyl}-1H-1,2,3-triazol-4-yl}methyl}pyrimidine-2,4(1H,3H)-dione

Base Information

Chemical Name:1-{{1-{(2Z)-2-phenyl-2-[(phenylmethoxy)imino]ethyl}-1H-1,2,3-triazol-4-yl}methyl}pyrimidine-2,4(1H,3H)-dione
CAS No.:1357381-05-5
Molecular Formula:C₂₂H₂₀N₆O₃
Molecular Weight:416.439
Hs Code.:

Synonyms:1-{{1-{(2Z)-2-phenyl-2-[(phenylmethoxy)imino]ethyl}-1H-1,2,3-triazol-4-yl}methyl}pyrimidine-2,4(1H,3H)-dione

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Chemical Property of 1-{{1-{(2Z)-2-phenyl-2-[(phenylmethoxy)imino]ethyl}-1H-1,2,3-triazol-4-yl}methyl}pyrimidine-2,4(1H,3H)-dione

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Technology Process of 1-{{1-{(2Z)-2-phenyl-2-[(phenylmethoxy)imino]ethyl}-1H-1,2,3-triazol-4-yl}methyl}pyrimidine-2,4(1H,3H)-dione

There total 4 articles about 1-{{1-{(2Z)-2-phenyl-2-[(phenylmethoxy)imino]ethyl}-1H-1,2,3-triazol-4-yl}methyl}pyrimidine-2,4(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1357380-88-1
C₁₅H₁₄N₆O₃

: 1357381-05-5
1-{{1-{(2Z)-2-phenyl-2-[(phenylmethoxy)imino]ethyl}-1H-1,2,3-triazol-4-yl}methyl}pyrimidine-2,4(1H,3H)-dione

Guidance literature:: With potassium hydroxide; In water; dimethyl sulfoxide; at 20 ℃;
DOI:10.1002/hlca.201100189

Reference yield:

: 40814-66-2
(Z)-2-chloro-1-phenylethan-1-one oxime

: 1357381-05-5
1-{{1-{(2Z)-2-phenyl-2-[(phenylmethoxy)imino]ethyl}-1H-1,2,3-triazol-4-yl}methyl}pyrimidine-2,4(1H,3H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / water; acetone / 12 h / 20 °C

2: copper(l) iodide / tetrahydrofuran; water / Reflux

3: potassium hydroxide / water; dimethyl sulfoxide / 20 °C

With copper(l) iodide; sodium azide; potassium hydroxide; In tetrahydrofuran; water; dimethyl sulfoxide; acetone; 2: Huisgen cycloaddition;
DOI:10.1002/hlca.201100189

Reference yield:

: 532-27-4,108321-66-0,164322-25-2
1-chloroacetophenone

: 1357381-05-5
1-{{1-{(2Z)-2-phenyl-2-[(phenylmethoxy)imino]ethyl}-1H-1,2,3-triazol-4-yl}methyl}pyrimidine-2,4(1H,3H)-dione

Guidance literature:: Multi-step reaction with 4 steps

1: hydroxylamine hydrochloride; potassium hydroxide / ethanol; water / 6 h / 20 °C

2: sodium azide / water; acetone / 12 h / 20 °C

3: copper(l) iodide / tetrahydrofuran; water / Reflux

4: potassium hydroxide / water; dimethyl sulfoxide / 20 °C

With copper(l) iodide; sodium azide; hydroxylamine hydrochloride; potassium hydroxide; In tetrahydrofuran; ethanol; water; dimethyl sulfoxide; acetone; 3: Huisgen cycloaddition;
DOI:10.1002/hlca.201100189