N¹,N¹²-diethyl-6-hydroxy-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

Base Information

• Chemical Name: N¹,N¹²-diethyl-6-hydroxy-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine
• CAS No.: 852057-85-3
• Molecular Formula: C₅₀H₇₄N₄O₉S₄
• Molecular Weight: 1003.42

Synonyms:N¹,N¹²-diethyl-6-hydroxy-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

Chemical Property of N¹,N¹²-diethyl-6-hydroxy-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

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Technology Process of N¹,N¹²-diethyl-6-hydroxy-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

There total 2 articles about N¹,N¹²-diethyl-6-hydroxy-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(2-bromoethyl)oxirane (13287-42-8) + N,N'-bis(mesitylenesulfonyl)-N-ethyl-1,3-diaminopropane (206991-72-2) → N1,N12-diethyl-6-hydroxy-N1,N4,N9,N12-tetrakis(mesitylenesulfonyl)spermine (852057-85-3)

Guidance literature:

N,N'-bis(mesitylenesulfonyl)-N-ethyl-1,3-diaminopropane; With sodium hydride; In N,N-dimethyl-formamide; for 0.5h;

(2-bromoethyl)oxirane; In N,N-dimethyl-formamide; at 70 ℃; for 18h;

DOI:10.1021/jm050024m

Reference yield:

N,N'-bis(mesitylenesulfonyl)-N-(3,4-epoxybutyl)-N'-ethyl-1,3-diaminopropane + N,N'-bis(mesitylenesulfonyl)-N-ethyl-1,3-diaminopropane (206991-72-2) → N1,N12-diethyl-6-hydroxy-N1,N4,N9,N12-tetrakis(mesitylenesulfonyl)spermine (852057-85-3)

Guidance literature:

at 70 ℃;

Reference yield: 61.0%

N1,N12-diethyl-6-hydroxy-N1,N4,N9,N12-tetrakis(mesitylenesulfonyl)spermine (852057-85-3) + p-toluenesulfonyl chloride (98-59-9) → N1,N12-diethyl-N1,N4,N9,N12-tetrakis(mesitylenesulfonyl)-6-(p-toluenesulfonato)spermine (852057-86-4)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1021/jm050024m

upstream raw materials:

(2-bromoethyl)oxirane

N,N'-bis(mesitylenesulfonyl)-N-ethyl-1,3-diaminopropane

Downstream raw materials:

N¹,N¹²-diethyl-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)-6-(p-toluenesulfonato)spermine

6-amino-N¹,N¹²-diethyl-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

N¹,N¹²-diethyl-6-phthalimido-N¹,N⁴,N⁹,N¹²-tetrakis(mesitylenesulfonyl)spermine

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