2-CYANO-4-FLUOROBENZYL BROMIDE

Base Information

• Chemical Name: 2-CYANO-4-FLUOROBENZYL BROMIDE
• CAS No.: 217661-27-3
• Molecular Formula: C8H5BrFN
• Molecular Weight: 214.037
• Hs Code.: 2926909090
• Mol file: 217661-27-3.mol

Synonyms:2-Cyano-4-fluorobenzyl bromide;3-Fluoro-6-bromomethylbenzonitrile;2-(Bromomethyl)-5-fluorobenzonitrile;

Chemical Property of 2-CYANO-4-FLUOROBENZYL BROMIDE

Chemical Property:

• Vapor Pressure: 0.01mmHg at 25°C
• Melting Point: 64.9-65.9 °C
• Refractive Index: 1.564
• Boiling Point: 263.576 °C at 760 mmHg
• Flash Point: 113.207 °C
• PSA: 23.79000
• Density: 1.591 g/cm³
• LogP: 2.59228
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2-(Bromomethyl)-5-fluorobenzonitrile ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-CYANO-4-FLUOROBENZYL BROMIDE

There total 2 articles about 2-CYANO-4-FLUOROBENZYL BROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

3-fluoro-6-methylbenzonitrile (77532-79-7) → 2-(bromomethyl)-5-fluorobenzonitrile (217661-27-3)

Guidance literature:

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 20 ℃; for 8.16667h;

Reference yield:

→ 2-(bromomethyl)-5-fluorobenzonitrile (217661-27-3)

Guidance literature:

Reference yield: 97.0%

2-bromo-3-(4-fluorophenyl)-6,7-dihydro-1H-pyrrolo[3,2-c]pyridin-4(5H)-one + 2-(bromomethyl)-5-fluorobenzonitrile (217661-27-3) → 2-((2-bromo-3-(4-fluorophenyl)-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)methyl)-5-fluorobenzonitrile

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 0.333333h; Microwave irradiation;

upstream raw materials:

3-fluoro-6-methylbenzonitrile

Downstream raw materials:

2-((1,3-dioxoisoindolin-2-yl)methyl)-5-fluorobenzonitrile

2-((5-bromo-1,6-dihydro-1-isopropyl-2-(methylthio)-6-oxopyrimidin-4-yloxy)methyl)-5-fluorobenzonitrile

2-[3-(2-Butynyl)-4-oxo-2-(piperazin-1-yl)-3,4-dihydroimidazo[4,5-d]pyridazin-5-ylmethyl]-5-fluorobenzonitrile trifluoroacetate

2-(bromomethyl)-5-fluorobenzaldehyde

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