5-Fluoro-2-methylbenzonitrile

Base Information

Chemical Name:5-Fluoro-2-methylbenzonitrile
CAS No.:77532-79-7
Molecular Formula:C8H6FN
Molecular Weight:135.141
Hs Code.:29269090
Mol file:77532-79-7.mol

Synonyms:3-Fluoro-6-methylbenzonitrile;Benzonitrile, 5-fluoro-2-methyl-;2-Methy-5-fluorobenzonitrile;5-fluoro-2-methylbenzenecarbonitrile;

Suppliers and Price of 5-Fluoro-2-methylbenzonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-Fluoro-2-methylbenzonitrile
1g
$ 75.00

TRC
5-Fluoro-2-methylbenzonitrile
100mg
$ 45.00

TCI Chemical
5-Fluoro-2-methylbenzonitrile >98.0%(GC)
25g
$ 104.00

TCI Chemical
5-Fluoro-2-methylbenzonitrile >98.0%(GC)
5g
$ 35.00

SynQuest Laboratories
5-Fluoro-2-methylbenzonitrile 98%
10 g
$ 15.00

Sigma-Aldrich
5-Fluoro-2-methylbenzonitrile 98%
5g
$ 92.20

Oakwood
5-Fluoro-2-methylbenzonitrile 98%
1g
$ 10.00

Oakwood
5-Fluoro-2-methylbenzonitrile 98%
5g
$ 11.00

Oakwood
5-Fluoro-2-methylbenzonitrile 98%
25g
$ 32.00

Matrix Scientific
5-Fluoro-2-methylbenzonitrile 98%
100g
$ 110.00

Total 65 raw suppliers

Chemical Property of 5-Fluoro-2-methylbenzonitrile

Chemical Property:

Appearance/Colour:yellow low melting solid
Vapor Pressure:0.273mmHg at 25°C
Melting Point:43-45 °C(lit.)
Refractive Index:1.507
Boiling Point:203.8 °C at 760 mmHg
Flash Point:79.4 °C
PSA：23.79000
Density:1.11 g/cm³
LogP:2.00578
Storage Temp.:Room temperature.
Solubility.:soluble in Methanol

Purity/Quality:

99%, ^*data from raw suppliers

5-Fluoro-2-methylbenzonitrile ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi,T
Hazard Codes:Xi,T
Statements: 37/38-41
Safety Statements: 26-39

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Fluoro-2-methylbenzonitrile

There total 5 articles about 5-Fluoro-2-methylbenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 953422-44-1
C₈H₈FNO

: 77532-79-7
3-fluoro-6-methylbenzonitrile

Guidance literature:: With trifluoromethylsulfonic anhydride; In dichloromethane; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.07.135

Reference yield: 81.0%

: 175278-28-1
5-fluoro-2-methylbenzamide

: 77532-79-7
3-fluoro-6-methylbenzonitrile

Guidance literature:: 5-fluoro-2-methylbenzamide; With C₃₉H₄₅N₂; In acetonitrile; at 20 ℃; Schlenk technique; Glovebox; Inert atmosphere;

With phenylsilane; In acetonitrile; at 80 ℃; for 12h; Temperature; Schlenk technique; Inert atmosphere; Sealed tube;
DOI:10.1039/c9cc08413d

Reference yield: 77.0%

: 1422-53-3
2-bromo-4-fluorotoluene

: 55305-43-6
N-cyano-N-phenyl-p-toluenesulfonamide

: 77532-79-7
3-fluoro-6-methylbenzonitrile

Guidance literature:: 2-bromo-4-fluorotoluene; With magnesium; lithium chloride; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

N-cyano-N-phenyl-p-toluenesulfonamide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201003388