C₁₉H₁₇NOS

Base Information

Chemical Name:C₁₉H₁₇NOS
CAS No.:712273-24-0
Molecular Formula:C₁₉H₁₇NOS
Molecular Weight:307.416
Hs Code.:

Synonyms:C₁₉H₁₇NOS

Suppliers and Price of C₁₉H₁₇NOS

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₉H₁₇NOS

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₉H₁₇NOS

There total 7 articles about C₁₉H₁₇NOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 712273-23-9
2-benzenesulfinyl-3-(4-triisopropylsilanyloxy-pent-4-enyl)-1H-indole

: 712273-24-0
C₁₉H₁₇NOS

Guidance literature:: With 2,6-dimethylpyridine; trifluoromethanesulfonic acid anhydride; In dichloromethane; at -75 ℃; for 0.0333333h;
DOI:10.1021/ol0493406

Reference yield: 42.0%

: 863976-69-6
2-phenylsulfenyl-3-(4-triisopropylsilanyloxy-pent-4-enyl)-1H-indole

: 712273-24-0
C₁₉H₁₇NOS

Guidance literature:: With lutidine; oxy>iodo>benzene; In acetonitrile; at 0 ℃;
DOI:10.1016/j.tetlet.2004.04.182

Reference yield:

: 133-32-4
4-indol-3-yl-butyric acid

: 712273-24-0
C₁₉H₁₇NOS

Guidance literature:: Multi-step reaction with 6 steps

1.1: 79 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; 4-(dimethylamino)pyridine / CH₂Cl₂ / 6.5 h

2.1: 89 percent / HCl / dioxane / 0.08 h

3.1: 95 percent / diethyl ether; tetrahydrofuran / 1 h / 0 °C

4.1: 91 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 3 h / 0 °C

5.1: lithium diisopropylamide / hexane; tetrahydrofuran / 1 h / -78 °C

5.2: 54 percent / N,N'-dimethylpropyleneurea / hexane; tetrahydrofuran / 2.5 h / -78 - 20 °C

6.1: 76 percent / trifluoromethanesulfonic anhydride; 2,6-lutidine / CH₂Cl₂ / 0.03 h / -75 °C

With 2,6-dimethylpyridine; hydrogenchloride; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoromethanesulfonic acid anhydride; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; diethyl ether; hexane; dichloromethane; 6.1: Pummerer reaction;
DOI:10.1021/ol0493406