3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanal

Base Information

Chemical Name:3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanal
CAS No.:261364-66-3
Molecular Formula:C₂₃H₃₅NO₇
Molecular Weight:437.533
Hs Code.:

Synonyms:3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanal

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Chemical Property of 3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanal

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Technology Process of 3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanal

There total 5 articles about 3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 261364-65-2
3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanol

: 261364-66-3
3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanal

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃;
DOI:10.1021/jm990498j

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 261364-66-3
3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanal

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / CHCl₃ / 1.5 h / 20 °C

2: 96 percent / pyridine / CHCl₃ / 25 - 30 °C

3: 28 percent / diisopropylethylamine / CHCl₃ / Heating

4: 82 percent / aq. AcOH / tetrahydrofuran / 1 h / 20 °C

5: 97 percent / pyridinium chlorochromate / CH₂Cl₂ / 20 °C

With pyridine; acetic acid; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; chloroform; 1: Acylation / 2: Acylation / 3: Condensation / 4: desilylation / 5: Oxidation;
DOI:10.1021/jm990498j

Reference yield:

: 139115-91-6
2-(2-tert-butyloxycarbonylaminoethoxy)ethanol

: 261364-66-3
3-(2'-(2''-(2''-Boc-aminoethoxy)ethoxycarbonyloxy)-4',6'-dimethylphenyl)-3,3-dimethylpropanal

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / pyridine / CHCl₃ / 25 - 30 °C

2: 28 percent / diisopropylethylamine / CHCl₃ / Heating

3: 82 percent / aq. AcOH / tetrahydrofuran / 1 h / 20 °C

4: 97 percent / pyridinium chlorochromate / CH₂Cl₂ / 20 °C

With pyridine; acetic acid; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; chloroform; 1: Acylation / 2: Condensation / 3: desilylation / 4: Oxidation;
DOI:10.1021/jm990498j