4,7-diphenyl-1,10-phenanhroline-[1,2-dithiolato-1,2-dicarba-closo-dodecaborane⁽¹²⁾] platinum(II)

Base Information

• Chemical Name: 4,7-diphenyl-1,10-phenanhroline-[1,2-dithiolato-1,2-dicarba-closo-dodecaborane⁽¹²⁾] platinum(II)
• CAS No.: 203911-48-2
• Molecular Formula: C₂₆H₂₆B₁₀N₂PtS₂
• Molecular Weight: 733.828

Synonyms:4,7-diphenyl-1,10-phenanhroline-[1,2-dithiolato-1,2-dicarba-closo-dodecaborane⁽¹²⁾] platinum(II)

Chemical Property of 4,7-diphenyl-1,10-phenanhroline-[1,2-dithiolato-1,2-dicarba-closo-dodecaborane⁽¹²⁾] platinum(II)

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Technology Process of 4,7-diphenyl-1,10-phenanhroline-[1,2-dithiolato-1,2-dicarba-closo-dodecaborane⁽¹²⁾] platinum(II)

There total 3 articles about 4,7-diphenyl-1,10-phenanhroline-[1,2-dithiolato-1,2-dicarba-closo-dodecaborane⁽¹²⁾] platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1,2-dicarba-closo-dodecaborane-1,2-dithiol (23810-63-1) + dichlorido(4,7-diphenyl-1,10-phenanthroline)platinum(II) (35273-41-7) → 4,7-diphenyl-1,10-phenanhroline-[1,2-dithiolato-1,2-dicarba-closo-dodecaborane(12)] platinum(II) (203911-48-2)

Guidance literature:

With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In dichloromethane; 3.5 h; elem. anal.;

DOI:10.1021/ic980872q

Reference yield:

bathophenanthroline (1662-01-7) → 4,7-diphenyl-1,10-phenanhroline-[1,2-dithiolato-1,2-dicarba-closo-dodecaborane(12)] platinum(II) (203911-48-2)

Guidance literature:

Multi-step reaction with 2 steps

2: n-butyllithium / Inert atmosphere

With n-butyllithium;

DOI:10.1039/c4dt01929f

Reference yield:

dichlorido(4,7-diphenyl-1,10-phenanthroline)platinum(II) (35273-41-7) + 1,2-dithiol-1,2-closo-dicarbadodecarborane → 4,7-diphenyl-1,10-phenanhroline-[1,2-dithiolato-1,2-dicarba-closo-dodecaborane(12)] platinum(II) (203911-48-2)

Guidance literature:

With n-butyllithium; Inert atmosphere;

DOI:10.1039/c4dt01929f

upstream raw materials:

1,2-dicarba-closo-dodecaborane-1,2-dithiol

dichlorido(4,7-diphenyl-1,10-phenanthroline)platinum(II)

bathophenanthroline

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