2-[2,7-dichloro-3-oxo-6-(prop-2-ynyloxy)-3H-xanthen-9-yl]benzoic acid prop-2-ynyl ester

Base Information

Chemical Name:2-[2,7-dichloro-3-oxo-6-(prop-2-ynyloxy)-3H-xanthen-9-yl]benzoic acid prop-2-ynyl ester
CAS No.:1309362-32-0
Molecular Formula:C₂₆H₁₄Cl₂O₅
Molecular Weight:477.3
Hs Code.:

Synonyms:2-[2,7-dichloro-3-oxo-6-(prop-2-ynyloxy)-3H-xanthen-9-yl]benzoic acid prop-2-ynyl ester

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Chemical Property of 2-[2,7-dichloro-3-oxo-6-(prop-2-ynyloxy)-3H-xanthen-9-yl]benzoic acid prop-2-ynyl ester

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Technology Process of 2-[2,7-dichloro-3-oxo-6-(prop-2-ynyloxy)-3H-xanthen-9-yl]benzoic acid prop-2-ynyl ester

There total 1 articles about 2-[2,7-dichloro-3-oxo-6-(prop-2-ynyloxy)-3H-xanthen-9-yl]benzoic acid prop-2-ynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 18362-80-6
2,7-dichlorofluorescein

: 106-96-7
propargyl bromide

: 1309362-32-0
2-[2,7-dichloro-3-oxo-6-(prop-2-ynyloxy)-3H-xanthen-9-yl]benzoic acid prop-2-ynyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 6h; Inert atmosphere;
DOI:10.1039/c001922d

Reference yield: 65.0%

: 1309362-32-0
2-[2,7-dichloro-3-oxo-6-(prop-2-ynyloxy)-3H-xanthen-9-yl]benzoic acid prop-2-ynyl ester

: 1309362-33-1
2,7-dichloro-9-[(2-hydroxymethyl)phenyl]-6-(prop-2-ynyloxy)-3H-xanthen-3-one

Guidance literature:: 2-[2,7-dichloro-3-oxo-6-(prop-2-ynyloxy)-3H-xanthen-9-yl]benzoic acid prop-2-ynyl ester; With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 - 25 ℃; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In diethyl ether; hexane; dichloromethane; at 25 ℃; for 2h;
DOI:10.1039/c001922d