(1E)-(5,5-bis-(tert-butyldiphenylsiloxymethyl)cyclohex-2-enylidene)methyl acetate

Base Information

• Chemical Name: (1E)-(5,5-bis-(tert-butyldiphenylsiloxymethyl)cyclohex-2-enylidene)methyl acetate
• CAS No.: 928119-07-7
• Molecular Formula: C₄₃H₅₂O₄Si₂
• Molecular Weight: 689.054

Synonyms:(1E)-(5,5-bis-(tert-butyldiphenylsiloxymethyl)cyclohex-2-enylidene)methyl acetate

Chemical Property of (1E)-(5,5-bis-(tert-butyldiphenylsiloxymethyl)cyclohex-2-enylidene)methyl acetate

Chemical Property:

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Technology Process of (1E)-(5,5-bis-(tert-butyldiphenylsiloxymethyl)cyclohex-2-enylidene)methyl acetate

There total 1 articles about (1E)-(5,5-bis-(tert-butyldiphenylsiloxymethyl)cyclohex-2-enylidene)methyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

C41H48O2Si2 + acetic acid (64-19-7,77671-22-8) → (1E)-(5,5-bis-(tert-butyldiphenylsiloxymethyl)cyclohex-2-enylidene)methyl acetate (928119-07-7)

Guidance literature:

With dmap; P(p-C₆H₄F)3; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; In 1,4-dioxane; at 65 ℃; for 24h;

DOI:10.1021/ja067336e

Reference yield: 88.0%

(1E)-(5,5-bis-(tert-butyldiphenylsiloxymethyl)cyclohex-2-enylidene)methyl acetate (928119-07-7) → 3-bromo-5,5-bis-(tert-butyldiphenylsiloxymethyl)cyclohex-1-enecarbaldehyde

Guidance literature:

With N-Bromosuccinimide; In 1,4-dioxane; water; at 20 ℃; for 2h;

DOI:10.1021/ja067336e

Reference yield: 85.0%

(1E)-(5,5-bis-(tert-butyldiphenylsiloxymethyl)cyclohex-2-enylidene)methyl acetate (928119-07-7) → 1-formyl-5,5-bis-(tert-butyldiphenylsiloxymethyl)cyclohex-2-enyl acetate

Guidance literature:

With DMDO; In dichloromethane; acetone; at -40 - 20 ℃;

DOI:10.1021/ja067336e

upstream raw materials:

acetic acid

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