N-(2-bromo-4-methoxyphenyl)-N-methyl-2-(o-fluorophenyl)-pent-4-enamide

Base Information

Chemical Name:N-(2-bromo-4-methoxyphenyl)-N-methyl-2-(o-fluorophenyl)-pent-4-enamide
CAS No.:1222096-91-4
Molecular Formula:C₁₉H₁₉BrFNO₂
Molecular Weight:392.268
Hs Code.:

Synonyms:N-(2-bromo-4-methoxyphenyl)-N-methyl-2-(o-fluorophenyl)-pent-4-enamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-bromo-4-methoxyphenyl)-N-methyl-2-(o-fluorophenyl)-pent-4-enamide

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Technology Process of N-(2-bromo-4-methoxyphenyl)-N-methyl-2-(o-fluorophenyl)-pent-4-enamide

There total 1 articles about N-(2-bromo-4-methoxyphenyl)-N-methyl-2-(o-fluorophenyl)-pent-4-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₁₀ClFO

: 264909-78-6
2-bromo-4-methoxy-N-methylaniline

: 1222096-91-4
N-(2-bromo-4-methoxyphenyl)-N-methyl-2-(o-fluorophenyl)-pent-4-enamide

Guidance literature:: C₁₁H₁₀ClFO; 2-bromo-4-methoxy-N-methylaniline; With triethylamine; In dichloromethane; at 0 - 20 ℃; for 16h; Inert atmosphere;

In mineral oil;
DOI:10.1021/ol1003093

Reference yield: 90.0%

: 1222096-91-4
N-(2-bromo-4-methoxyphenyl)-N-methyl-2-(o-fluorophenyl)-pent-4-enamide

: 1222097-05-3
(S)-3-allyl-3-(2-fluorophenyl)-5-methoxy-1-methylindolin-2-one

Guidance literature:: With chloro[(1,2,3-n)-3-phenyl-2-propenyl][4S,5S-1,3-bis[2-(3-pentyl)-naphthalen-1-yl]-4,5-di-(4-methoxy-phenyl)-4,5-dihydro-imidazol-2-ylidene]palladium(II); sodium t-butanolate; In 1,2-dimethoxyethane; at 23 ℃; for 16h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol1003093

Reference yield:

: 1222096-91-4
N-(2-bromo-4-methoxyphenyl)-N-methyl-2-(o-fluorophenyl)-pent-4-enamide

: 3-allyl-3-(2-fluorophenyl)-5-methoxy-1-methylindolin-2-one

Guidance literature:: With bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium t-butanolate; In 1,2-dimethoxyethane; at 50 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol1003093