1-(1,3-dioxolan-2-ylmethyl)cyclohexanecarbonitrile

Base Information

• Chemical Name: 1-(1,3-dioxolan-2-ylmethyl)cyclohexanecarbonitrile
• CAS No.: 1001024-20-9
• Molecular Formula: C₁₁H₁₇NO₂
• Molecular Weight: 195.261
• Mol file: 1001024-20-9.mol

Synonyms:1-(1,3-dioxolan-2-ylmethyl)cyclohexanecarbonitrile

Chemical Property of 1-(1,3-dioxolan-2-ylmethyl)cyclohexanecarbonitrile

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(1,3-dioxolan-2-ylmethyl)cyclohexanecarbonitrile

There total 1 articles about 1-(1,3-dioxolan-2-ylmethyl)cyclohexanecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

ethylene glycol (107-21-1) → 1-(1,3-dioxolan-2-ylmethyl)cyclohexanecarbonitrile (1001024-20-9)

Guidance literature:

1-allylcyclohexane-1-nitrile; With ozone; In ethylene glycol; tert-butyl alcohol; at 20 ℃;

With dimethylsulfide; In ethylene glycol; tert-butyl alcohol; at 25 ℃; for 1h;

ethylene glycol; methanesulfonic acid; In cyclohexane;

Reference yield: 85.0%

1-(1,3-dioxolan-2-ylmethyl)cyclohexanecarbonitrile (1001024-20-9) → 1-aminomethyl-1-(1,3-dioxolan-2-yImethyl)cyclohexane

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 2h;

Reference yield: 82.0%

1-(1,3-dioxolan-2-ylmethyl)cyclohexanecarbonitrile (1001024-20-9) → (1-cyanocyclohexyl)-acetic acid (133481-09-1)

Guidance literature:

1-(1,3-dioxolan-2-ylmethyl)cyclohexanecarbonitrile; With ozone; In acetic acid butyl ester; at 25 ℃;

With dimethylsulfide; In acetic acid butyl ester; at 35 ℃; for 2h;

upstream raw materials:

ethylene glycol

Downstream raw materials:

hydroxyethyl (1-cyano-cyclohexyl)acetate

(1-cyanocyclohexyl)-acetic acid

Refernces