3-[benzyl-(2-chloro-5-nitro-pyrimidin-4-yl)-amino]-propanoic acid ethyl ester

Base Information

• Chemical Name: 3-[benzyl-(2-chloro-5-nitro-pyrimidin-4-yl)-amino]-propanoic acid ethyl ester
• CAS No.: 1062244-31-8
• Molecular Formula: C₁₆H₁₇ClN₄O₄
• Molecular Weight: 364.788

Synonyms:3-[benzyl-(2-chloro-5-nitro-pyrimidin-4-yl)-amino]-propanoic acid ethyl ester

Chemical Property of 3-[benzyl-(2-chloro-5-nitro-pyrimidin-4-yl)-amino]-propanoic acid ethyl ester

Chemical Property:

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Technology Process of 3-[benzyl-(2-chloro-5-nitro-pyrimidin-4-yl)-amino]-propanoic acid ethyl ester

There total 2 articles about 3-[benzyl-(2-chloro-5-nitro-pyrimidin-4-yl)-amino]-propanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl-3-benzylamino propionate (23583-21-3) + 2,4-Dichloro-5-nitropyrimidine (49845-33-2) → 3-[benzyl-(2-chloro-5-nitro-pyrimidin-4-yl)-amino]-propanoic acid ethyl ester (1062244-31-8)

Guidance literature:

With potassium hydrogencarbonate; In diethyl ether; water; at 0 - 20 ℃; for 3h;

Reference yield:

→ 3-[benzyl-(2-chloro-5-nitro-pyrimidin-4-yl)-amino]-propanoic acid ethyl ester (1062244-31-8)

Guidance literature:

Reference yield:

3-[benzyl-(2-chloro-5-nitro-pyrimidin-4-yl)-amino]-propanoic acid ethyl ester (1062244-31-8) → 9-benzyl-2-chloro-5,7,8,9-tetrahydro-pyrimido[4,5-b][1,4]diazepin-6-one (1062244-34-1)

Guidance literature:

With hydrogenchloride; tin(ll) chloride; In ethanol; at 60 ℃; for 2h;

upstream raw materials:

ethyl-3-benzylamino propionate

2,4-Dichloro-5-nitropyrimidine

Downstream raw materials:

9-benzyl-2-chloro-5,7,8,9-tetrahydro-pyrimido[4,5-b][1,4]diazepin-6-one

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