dibenzyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl phosphate

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Chemical Name:dibenzyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl phosphate
CAS No.:1224950-18-8
Molecular Formula:C₃₇H₃₉N₂O₆P
Molecular Weight:638.7
Hs Code.:

Synonyms:dibenzyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl phosphate

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Chemical Property of dibenzyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl phosphate

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Technology Process of dibenzyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl phosphate

There total 7 articles about dibenzyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 990-91-0
dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate

: 1224948-06-4
1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)cyclohexane-cis-1,4-diol

: 1224950-18-8
dibenzyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl phosphate

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 15h; Cooling with ice;

Reference yield:

: 70097-74-4
8-ethynyl-1,4-dioxaspiro[4.5]decan-8-ol

: 1224950-18-8
dibenzyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl phosphate

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.92 h / -72 °C

1.2: 0.58 h / -72 °C

2.1: manganese(IV) oxide / dichloromethane / 15 h / 20 °C

3.1: triethylamine / ethanol / 0.5 h / 20 °C

3.2: 15 h / 20 °C

4.1: hydrogenchloride; water / tetrahydrofuran / 15 h / 20 °C

4.2: 0 °C

5.1: sodium tetrahydroborate; methanol / 2 h / 20 °C

6.1: sodium hydride / tetrahydrofuran; mineral oil / 15 h / 20 °C / Cooling with ice

With hydrogenchloride; methanol; manganese(IV) oxide; sodium tetrahydroborate; n-butyllithium; water; sodium hydride; triethylamine; In tetrahydrofuran; ethanol; hexane; dichloromethane; mineral oil;

Reference yield:

: 1224949-51-2
8-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-1,4-dioxaspiro[4.5]decan-8-ol

: 1224950-18-8
dibenzyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; water / tetrahydrofuran / 15 h / 20 °C

1.2: 0 °C

2.1: sodium tetrahydroborate; methanol / 2 h / 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 15 h / 20 °C / Cooling with ice

With hydrogenchloride; methanol; sodium tetrahydroborate; water; sodium hydride; In tetrahydrofuran; mineral oil;