(+)-(2R,3R,4S,7S)-3-(((3R,4R)-3,4-dihydroxypentanoyl)oxy)-7-(3-hydroxyphenyl)-7-methoxy-2,4-dimethylheptanoic acid

Base Information

Chemical Name:(+)-(2R,3R,4S,7S)-3-(((3R,4R)-3,4-dihydroxypentanoyl)oxy)-7-(3-hydroxyphenyl)-7-methoxy-2,4-dimethylheptanoic acid
CAS No.:1224952-48-0
Molecular Formula:C₂₁H₃₂O₈
Molecular Weight:412.48
Hs Code.:

Synonyms:(+)-(2R,3R,4S,7S)-3-(((3R,4R)-3,4-dihydroxypentanoyl)oxy)-7-(3-hydroxyphenyl)-7-methoxy-2,4-dimethylheptanoic acid

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Chemical Property of (+)-(2R,3R,4S,7S)-3-(((3R,4R)-3,4-dihydroxypentanoyl)oxy)-7-(3-hydroxyphenyl)-7-methoxy-2,4-dimethylheptanoic acid

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Technology Process of (+)-(2R,3R,4S,7S)-3-(((3R,4R)-3,4-dihydroxypentanoyl)oxy)-7-(3-hydroxyphenyl)-7-methoxy-2,4-dimethylheptanoic acid

There total 40 articles about (+)-(2R,3R,4S,7S)-3-(((3R,4R)-3,4-dihydroxypentanoyl)oxy)-7-(3-hydroxyphenyl)-7-methoxy-2,4-dimethylheptanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: (+)-(2R,3R,4S,7S)-3-(((3R,4R)-3,4-bis((tert-butyldimethylsilyl)oxy)pentanoyl)oxy)-7-(3-hydroxyphenyl)-7-methoxy-2,4-dimethylheptanoic acid

: 1224952-48-0
(+)-(2R,3R,4S,7S)-3-(((3R,4R)-3,4-dihydroxypentanoyl)oxy)-7-(3-hydroxyphenyl)-7-methoxy-2,4-dimethylheptanoic acid

Guidance literature:: (+)-(2R,3R,4S,7S)-3-(((3R,4R)-3,4-bis((tert-butyldimethylsilyl)oxy)pentanoyl)oxy)-7-(3-hydroxyphenyl)-7-methoxy-2,4-dimethylheptanoic acid; With pyridine hydrogenfluoride; In tetrahydrofuran; at 0 - 20 ℃; for 38h; Inert atmosphere;

With Trimethylmethoxysilane; In tetrahydrofuran; at 0 - 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1021/acs.joc.6b03060

Reference yield: 67.0%

: 1450899-63-4
(2R,3R,4S,7S)-allyl-3-((3R,4R)-3,4-bis(tert-butyldimethylsilyloxy)pentanoyloxy)-7-(3-(tert-butyldimethylsilyloxy)phenyl)-7-methoxy-2,4-dimethylheptanoate

: 1224952-48-0
(+)-(2R,3R,4S,7S)-3-(((3R,4R)-3,4-dihydroxypentanoyl)oxy)-7-(3-hydroxyphenyl)-7-methoxy-2,4-dimethylheptanoic acid

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere; Darkness;
DOI:10.1021/jo401248n