C₁₆H₁₂O₆

Base Information

Chemical Name:C₁₆H₁₂O₆
CAS No.:1312609-87-2
Molecular Formula:C₁₆H₁₂O₆
Molecular Weight:300.268
Hs Code.:

C<sub>16</sub>H<sub>12</sub>O<sub>6</sub>

Synonyms:C₁₆H₁₂O₆

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Chemical Property of C₁₆H₁₂O₆

Chemical Property:

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Technology Process of C₁₆H₁₂O₆

There total 10 articles about C₁₆H₁₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1312609-85-0
C₁₉H₁₈O₆

: 1312609-87-2
C₁₆H₁₂O₆

Guidance literature:: C₁₉H₁₈O₆; With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 17h;

With hydrogenchloride; In tetrahydrofuran; water; pH=2;

Reference yield:

: 148-53-8
3-methoxy-2-hydroxybenzaldehyde

: 1312609-87-2
C₁₆H₁₂O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: pyridine / 24 h / 20 °C

2.1: nitric acid; sulfuric acid / 0.08 h / -40 °C

3.1: sodium hydroxide / water / 0.08 h

3.2: 85 °C

3.3: pH 2

4.1: water; hydrogen bromide; acetic acid / 4 h / Reflux

5.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 2068.65 Torr

6.1: sodium nitrite; hydrogen bromide / water / 2 h / 0 °C

6.2: 0 - 20 °C

7.1: sulfuric acid / 16 h / Reflux

8.1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

8.2: 12 h / 70 °C

9.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 10 h / 80 °C / Inert atmosphere

10.1: water; lithium hydroxide / tetrahydrofuran / 17 h / 20 °C

10.2: pH 2

With pyridine; sulfuric acid; water; hydrogen bromide; hydrogen; nitric acid; sodium carbonate; caesium carbonate; acetic acid; sodium hydroxide; lithium hydroxide; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide; toluene; 9.1: Suzuki Coupling;

Reference yield:

: 7150-01-8
2-acetoxy-3-methoxybenzaldehyde

: 1312609-87-2
C₁₆H₁₂O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: nitric acid; sulfuric acid / 0.08 h / -40 °C

2.1: sodium hydroxide / water / 0.08 h

2.2: 85 °C

2.3: pH 2

3.1: water; hydrogen bromide; acetic acid / 4 h / Reflux

4.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 2068.65 Torr

5.1: sodium nitrite; hydrogen bromide / water / 2 h / 0 °C

5.2: 0 - 20 °C

6.1: sulfuric acid / 16 h / Reflux

7.1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

7.2: 12 h / 70 °C

8.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 10 h / 80 °C / Inert atmosphere

9.1: water; lithium hydroxide / tetrahydrofuran / 17 h / 20 °C

9.2: pH 2

With sulfuric acid; water; hydrogen bromide; hydrogen; nitric acid; sodium carbonate; caesium carbonate; acetic acid; sodium hydroxide; lithium hydroxide; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide; toluene; 8.1: Suzuki Coupling;