phenyl 3,4-di-O-benzyl-2-O-(2-naphthylmethyl)-1-thio-α-L-rhamnopyranoside

Base Information

Chemical Name:phenyl 3,4-di-O-benzyl-2-O-(2-naphthylmethyl)-1-thio-α-L-rhamnopyranoside
CAS No.:940006-59-7
Molecular Formula:C₃₇H₃₆O₄S
Molecular Weight:576.756
Hs Code.:

Synonyms:phenyl 3,4-di-O-benzyl-2-O-(2-naphthylmethyl)-1-thio-α-L-rhamnopyranoside

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Chemical Property of phenyl 3,4-di-O-benzyl-2-O-(2-naphthylmethyl)-1-thio-α-L-rhamnopyranoside

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Technology Process of phenyl 3,4-di-O-benzyl-2-O-(2-naphthylmethyl)-1-thio-α-L-rhamnopyranoside

There total 8 articles about phenyl 3,4-di-O-benzyl-2-O-(2-naphthylmethyl)-1-thio-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 939-26-4
2-bromomethylnaphthyl bromide

: 172296-66-1
Phenyl 3,4-di-O-benzyl-1-thio-α-L-rhamnopyranoside

: 940006-59-7
phenyl 3,4-di-O-benzyl-2-O-(2-naphthylmethyl)-1-thio-α-L-rhamnopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1021/jo062411p

Reference yield: 78.0%

: 1428344-38-0
C₂₃H₂₄O₄S

: 100-39-0
benzyl bromide

: 940006-59-7
phenyl 3,4-di-O-benzyl-2-O-(2-naphthylmethyl)-1-thio-α-L-rhamnopyranoside

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1021/ol400430p

Reference yield:

: 1214-98-8,105026-40-2,127061-11-4,131724-82-8
phenyl 1-thio-α-L-rhamnopyranose

: 940006-59-7
phenyl 3,4-di-O-benzyl-2-O-(2-naphthylmethyl)-1-thio-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: camphor-10-sulfonic acid / methanol / Reflux

2: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 0 - 20 °C

3: trifluoroacetic acid / water; dichloromethane / 20 °C

4: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 0 - 20 °C

With camphor-10-sulfonic acid; tetra-(n-butyl)ammonium iodide; sodium hydride; trifluoroacetic acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol400430p