(Z)-2-[3-(benzyloxy)-4-isopropoxyphenethyl]-2'-(4-fluoro-3-nitrostyryl)-4-isopropoxy-4'-methoxybiphenyl

Base Information

Chemical Name:(Z)-2-[3-(benzyloxy)-4-isopropoxyphenethyl]-2'-(4-fluoro-3-nitrostyryl)-4-isopropoxy-4'-methoxybiphenyl
CAS No.:1312673-45-2
Molecular Formula:C₄₂H₄₂FNO₆
Molecular Weight:675.797
Hs Code.:

Synonyms:(Z)-2-[3-(benzyloxy)-4-isopropoxyphenethyl]-2'-(4-fluoro-3-nitrostyryl)-4-isopropoxy-4'-methoxybiphenyl

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Chemical Property of (Z)-2-[3-(benzyloxy)-4-isopropoxyphenethyl]-2'-(4-fluoro-3-nitrostyryl)-4-isopropoxy-4'-methoxybiphenyl

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Technology Process of (Z)-2-[3-(benzyloxy)-4-isopropoxyphenethyl]-2'-(4-fluoro-3-nitrostyryl)-4-isopropoxy-4'-methoxybiphenyl

There total 7 articles about (Z)-2-[3-(benzyloxy)-4-isopropoxyphenethyl]-2'-(4-fluoro-3-nitrostyryl)-4-isopropoxy-4'-methoxybiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42564-51-2
4-fluoro-3-nitrobenzaldehyde

: 1312673-45-2
(Z)-2-[3-(benzyloxy)-4-isopropoxyphenethyl]-2'-(4-fluoro-3-nitrostyryl)-4-isopropoxy-4'-methoxybiphenyl

: (E)-2-[3-(benzyloxy)-4-isopropoxyphenethyl]-2'-(4-fluoro-3-nitrostyryl)-4-isopropoxy-4'-methoxybiphenyl

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate / methanol

2: phosphorus tribromide / toluene

3: toluene

4: sodium carbonate / dichloromethane; water / 24 h / 40 °C

With sodium tetrahydroborate; phosphorus tribromide; sodium carbonate; In methanol; dichloromethane; water; toluene; 4: Wittig reaction;
DOI:10.1002/ejoc.201001412

Reference yield:

: 1312673-44-1
2'-[3-(benzyloxy)-4-isopropoxyphenethyl]-4'-isopropoxy-4-methoxybiphenyl-2-carbaldehyde

: 288404-79-5
4-fluoro-3-nitrobenzyltriphenylphosphonium bromide

: 1312673-45-2
(Z)-2-[3-(benzyloxy)-4-isopropoxyphenethyl]-2'-(4-fluoro-3-nitrostyryl)-4-isopropoxy-4'-methoxybiphenyl

: (E)-2-[3-(benzyloxy)-4-isopropoxyphenethyl]-2'-(4-fluoro-3-nitrostyryl)-4-isopropoxy-4'-methoxybiphenyl

Guidance literature:: With sodium carbonate; In dichloromethane; water; at 40 ℃; for 24h; optical yield given as %de;
DOI:10.1002/ejoc.201001412

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 1312673-45-2
(Z)-2-[3-(benzyloxy)-4-isopropoxyphenethyl]-2'-(4-fluoro-3-nitrostyryl)-4-isopropoxy-4'-methoxybiphenyl

: (E)-2-[3-(benzyloxy)-4-isopropoxyphenethyl]-2'-(4-fluoro-3-nitrostyryl)-4-isopropoxy-4'-methoxybiphenyl

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid; nitric acid

2: sodium tetrahydroborate / methanol

3: phosphorus tribromide / toluene

4: toluene

5: sodium carbonate / dichloromethane; water / 24 h / 40 °C

With sodium tetrahydroborate; sulfuric acid; nitric acid; phosphorus tribromide; sodium carbonate; In methanol; dichloromethane; water; toluene; 5: Wittig reaction;
DOI:10.1002/ejoc.201001412