2'-[3-(benzyloxy)-4-isopropoxyphenethyl]-4'-isopropoxy-4-methoxybiphenyl-2-carbaldehyde

Base Information

Chemical Name:2'-[3-(benzyloxy)-4-isopropoxyphenethyl]-4'-isopropoxy-4-methoxybiphenyl-2-carbaldehyde
CAS No.:1312673-44-1
Molecular Formula:C₃₅H₃₈O₅
Molecular Weight:538.684
Hs Code.:

Synonyms:2'-[3-(benzyloxy)-4-isopropoxyphenethyl]-4'-isopropoxy-4-methoxybiphenyl-2-carbaldehyde

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Chemical Property of 2'-[3-(benzyloxy)-4-isopropoxyphenethyl]-4'-isopropoxy-4-methoxybiphenyl-2-carbaldehyde

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Technology Process of 2'-[3-(benzyloxy)-4-isopropoxyphenethyl]-4'-isopropoxy-4-methoxybiphenyl-2-carbaldehyde

There total 6 articles about 2'-[3-(benzyloxy)-4-isopropoxyphenethyl]-4'-isopropoxy-4-methoxybiphenyl-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1312673-43-0
2-(benzyloxy)-4-(2-bromo-5-isopropoxyphenethyl)-1-isopropoxybenzene

: 139962-95-1
2-formyl-4-methoxyphenylboronic acid

: 1312673-44-1
2'-[3-(benzyloxy)-4-isopropoxyphenethyl]-4'-isopropoxy-4-methoxybiphenyl-2-carbaldehyde

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane; ethanol; water; for 24h; Reflux;
DOI:10.1002/ejoc.201001412

Reference yield:

: 2-(benzyloxy)-4-(2-bromo-5-isopropoxystyryl)-1-isopropoxybenzene

: 1312673-44-1
2'-[3-(benzyloxy)-4-isopropoxyphenethyl]-4'-isopropoxy-4-methoxybiphenyl-2-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: Wilkinson's catalyst; hydrogen / tetrahydrofuran; tert-butyl alcohol / 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; ethanol; water / 24 h / Reflux

With Wilkinson's catalyst; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; water; tert-butyl alcohol; 2: Suzuki reaction;
DOI:10.1002/ejoc.201001412

Reference yield:

: 98015-07-7
2-Bromo-5-methoxybenzaldehyde ethylene glycol acetal

: 1312673-44-1
2'-[3-(benzyloxy)-4-isopropoxyphenethyl]-4'-isopropoxy-4-methoxybiphenyl-2-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium / tetrahydrofuran

2: hydrogenchloride; water

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; ethanol; water / 24 h / Reflux

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; water; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; water; 3: Suzuki reaction;
DOI:10.1002/ejoc.201001412