2-Methyl-propane-2-sulfinic acid [1-((S)-2-hydroxy-2-phenyl-ethyl)-2,2-dimethyl-prop-(E)-ylidene]-amide

Base Information

• Chemical Name: 2-Methyl-propane-2-sulfinic acid [1-((S)-2-hydroxy-2-phenyl-ethyl)-2,2-dimethyl-prop-(E)-ylidene]-amide
• CAS No.: 606954-72-7
• Molecular Formula: C₁₇H₂₇NO₂S
• Molecular Weight: 309.473

Synonyms:2-Methyl-propane-2-sulfinic acid [1-((S)-2-hydroxy-2-phenyl-ethyl)-2,2-dimethyl-prop-(E)-ylidene]-amide

Chemical Property of 2-Methyl-propane-2-sulfinic acid [1-((S)-2-hydroxy-2-phenyl-ethyl)-2,2-dimethyl-prop-(E)-ylidene]-amide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Methyl-propane-2-sulfinic acid [1-((S)-2-hydroxy-2-phenyl-ethyl)-2,2-dimethyl-prop-(E)-ylidene]-amide

There total 1 articles about 2-Methyl-propane-2-sulfinic acid [1-((S)-2-hydroxy-2-phenyl-ethyl)-2,2-dimethyl-prop-(E)-ylidene]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzaldehyde (100-52-7) + (RS)-N-(3,3-dimethylbutan-2-ylidene)-2-methylpropane-2-sulfinamide (221375-58-2) → 2-Methyl-propane-2-sulfinic acid [1-((S)-2-hydroxy-2-phenyl-ethyl)-2,2-dimethyl-prop-(E)-ylidene]-amide (606954-72-7) + 2-Methyl-propane-2-sulfinic acid [1-((R)-2-hydroxy-2-phenyl-ethyl)-2,2-dimethyl-prop-(E)-ylidene]-amide

Guidance literature:

(R_S)-N-(3,3-dimethylbutan-2-ylidene)-2-methylpropane-2-sulfinamide; With n-butyllithium; diisopropylamine; In tetrahydrofuran; pentane; at -78 ℃; for 0.75h;

With magnesium bromide; In tetrahydrofuran; pentane; at -78 ℃; for 0.75h;

benzaldehyde; In tetrahydrofuran; pentane; at -78 ℃; for 1h; Title compound not separated from byproducts;

DOI:10.1021/ja0363462

Reference yield: 95.0%

2-Methyl-propane-2-sulfinic acid [1-((S)-2-hydroxy-2-phenyl-ethyl)-2,2-dimethyl-prop-(E)-ylidene]-amide (606954-72-7) → 2-Methyl-propane-2-sulfinic acid [(S)-1-((S)-2-hydroxy-2-phenyl-ethyl)-2,2-dimethyl-propyl]-amide

Guidance literature:

With lithium triethylborohydride; In tetrahydrofuran; at -78 ℃; for 3h;

DOI:10.1021/ja0363462

Reference yield:

2-Methyl-propane-2-sulfinic acid [1-((S)-2-hydroxy-2-phenyl-ethyl)-2,2-dimethyl-prop-(E)-ylidene]-amide (606954-72-7) → 2-Methyl-propane-2-sulfinic acid [(R)-1-((S)-2-hydroxy-2-phenyl-ethyl)-2,2-dimethyl-propyl]-amide + 2-Methyl-propane-2-sulfinic acid [(S)-1-((S)-2-hydroxy-2-phenyl-ethyl)-2,2-dimethyl-propyl]-amide

Guidance literature:

With benzo[1,3,2]dioxaborole; In tetrahydrofuran; at -10 ℃; for 20h;

DOI:10.1021/ja0363462

upstream raw materials:

benzaldehyde

(R_S)-N-(3,3-dimethylbutan-2-ylidene)-2-methylpropane-2-sulfinamide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 606954-72-7 2-Methyl-propane-2-sulfinic acid [1-((S)-2-hydroxy-2-phenyl-ethyl)-2,2-dimethyl-prop-(E)-ylidene]-amide

Send

Send

Metric Ton KG G Pound L ML

Send

Send