Technology Process of Ru(C6H5N2C5H4N)2((CH3CO)2CH)(1+)*ClO4(1-)=Ru(C6H5N2C5H4N)2((CH3CO)2CH)ClO4
There total 1 articles about Ru(C6H5N2C5H4N)2((CH3CO)2CH)(1+)*ClO4(1-)=Ru(C6H5N2C5H4N)2((CH3CO)2CH)ClO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
ammonia;
In
perchloric acid;
Ru complex refluxing in 1 M HClO4 for 1 h, filtering hot, aq. NH3 and ligand adding, heating on a steam bath for 3 h, aq. NaClO4 adding, cooling to room temp. overnight, solid filtering off, washing with water, drying in vacuo over P4O10 at room temp.; identified by elem. anal., UV and IR spectra;