tosylate de N-benzyloxycarbonyl ethanolamine-13C

Base Information

• Chemical Name: tosylate de N-benzyloxycarbonyl ethanolamine-13C
• CAS No.: 170745-64-9
• Molecular Formula: C₁₇H₁₉NO₅S
• Molecular Weight: 350.397
• Mol file: 170745-64-9.mol

Synonyms:tosylate de N-benzyloxycarbonyl ethanolamine-13C

Chemical Property of tosylate de N-benzyloxycarbonyl ethanolamine-13C

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of tosylate de N-benzyloxycarbonyl ethanolamine-13C

There total 1 articles about tosylate de N-benzyloxycarbonyl ethanolamine-13C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

p-toluenesulfonyl chloride (98-59-9) + N-benzyloxycarbonyl ethanolamine-13C → tosylate de N-benzyloxycarbonyl ethanolamine-13C (170745-64-9)

Guidance literature:

With pyridine; at 4 ℃;

DOI:10.1002/jlcr.2580360813

Reference yield: 61.0%

tosylate de N-benzyloxycarbonyl ethanolamine-13C (170745-64-9) → N-benzyloxycarbonyl 2-iodoethylamine-13C

Guidance literature:

With sodium iodide; In acetone; Heating;

DOI:10.1002/jlcr.2580360813

Reference yield:

tosylate de N-benzyloxycarbonyl ethanolamine-13C (170745-64-9) → N-benzyloxycarbonyl N'-diethylethylene diamine-13C (170745-66-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 61 percent / NaI / acetone / Heating

2: 95 percent / tetrahydrofuran / Heating

With sodium iodide; In tetrahydrofuran; acetone;

DOI:10.1002/jlcr.2580360813

upstream raw materials:

p-toluenesulfonyl chloride

Downstream raw materials:

N-benzyloxycarbonyl N'-diethylethylene diamine-13C