N-benzyloxycarbonyl N'-diethylethylene diamine-13C

Base Information

• Chemical Name: N-benzyloxycarbonyl N'-diethylethylene diamine-13C
• CAS No.: 170745-66-1
• Molecular Formula: C₁₄H₂₂N₂O₂
• Molecular Weight: 251.33
• Mol file: 170745-66-1.mol

Synonyms:

Chemical Property of N-benzyloxycarbonyl N'-diethylethylene diamine-13C

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-benzyloxycarbonyl N'-diethylethylene diamine-13C

There total 3 articles about N-benzyloxycarbonyl N'-diethylethylene diamine-13C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

diethylamine (109-89-7) + N-benzyloxycarbonyl 2-iodoethylamine-13C → N-benzyloxycarbonyl N'-diethylethylene diamine-13C (170745-66-1)

Guidance literature:

In tetrahydrofuran; Heating;

DOI:10.1002/jlcr.2580360813

Reference yield:

N-benzyloxycarbonyl ethanolamine-13C → N-benzyloxycarbonyl N'-diethylethylene diamine-13C (170745-66-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 78 percent / pyridine / 4 °C

2: 61 percent / NaI / acetone / Heating

3: 95 percent / tetrahydrofuran / Heating

With pyridine; sodium iodide; In tetrahydrofuran; acetone;

DOI:10.1002/jlcr.2580360813

Reference yield:

tosylate de N-benzyloxycarbonyl ethanolamine-13C (170745-64-9) → N-benzyloxycarbonyl N'-diethylethylene diamine-13C (170745-66-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 61 percent / NaI / acetone / Heating

2: 95 percent / tetrahydrofuran / Heating

With sodium iodide; In tetrahydrofuran; acetone;

DOI:10.1002/jlcr.2580360813

upstream raw materials:

diethylamine

tosylate de N-benzyloxycarbonyl ethanolamine-13C