6-METHYL-2-(3-METHYL-5-OXO-2,5-DIHYDRO-1H-PYRAZOL-1-YL)-4(3H)-PYRIMIDINONE

Base Information

• Chemical Name: 6-METHYL-2-(3-METHYL-5-OXO-2,5-DIHYDRO-1H-PYRAZOL-1-YL)-4(3H)-PYRIMIDINONE
• CAS No.: 53068-50-1
• Molecular Formula: C₉H₁₀N₄O₂
• Molecular Weight: 206.204
• Mol file: 53068-50-1.mol

Synonyms:6-methyl-2-(3-methyl-5-oxo-2,5-dihydropyrazol-1-yl)pyrimidin-4(1H)-one

Chemical Property of 6-METHYL-2-(3-METHYL-5-OXO-2,5-DIHYDRO-1H-PYRAZOL-1-YL)-4(3H)-PYRIMIDINONE

Chemical Property:

Purity/Quality:

6-METHYL-2-(3-METHYL-5-OXO-2,5-DIHYDRO-1H-PYRAZOL-1-YL)-4(3H)-PYRIMIDINONE 95.00% ^*data from reagent suppliers

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Technology Process of 6-METHYL-2-(3-METHYL-5-OXO-2,5-DIHYDRO-1H-PYRAZOL-1-YL)-4(3H)-PYRIMIDINONE

There total 3 articles about 6-METHYL-2-(3-METHYL-5-OXO-2,5-DIHYDRO-1H-PYRAZOL-1-YL)-4(3H)-PYRIMIDINONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

2-hydrazino-6-methylpyrimidin-4(3H)-one (37893-08-6) + ethyl acetoacetate (141-97-9) → 6-methyl-2-(3-methyl-5-oxo-2,5-dihydropyrazol-1-yl)pyrimidin-4(1H)-one (53068-50-1)

Guidance literature:

In water; for 1h; Reflux;

DOI:10.1134/S1070363209070214

Reference yield:

(2,4,6-trioxo-1,2,3,4,5,6-hexahydropyrimidin-5-yl)[2-(5-hydroxy-3-methylpyrazol-1-yl)-6-methyl-4-oxo-3,4-dihydropyrimidin-5-yl]phenylmethane (1206694-35-0) → BARBITURIC ACID (67-52-7,944357-77-1) + 6-methyl-2-(3-methyl-5-oxo-2,5-dihydropyrazol-1-yl)pyrimidin-4(1H)-one (53068-50-1) + benzaldehyde (100-52-7)

Guidance literature:

With water;

DOI:10.1134/S1070363209070214

Reference yield:

→ 6-methyl-2-(3-methyl-5-oxo-2,5-dihydro-pyrazol-1-yl)-3H-pyrimidin-4-one (53068-50-1)

Guidance literature:

Aminoguanidin-bicarbonat: 1) Acetoacetamid (Diketen+NH4OH) 2) Methylacetoacetat/NaOMe;

upstream raw materials:

(2,4,6-trioxo-1,2,3,4,5,6-hexahydropyrimidin-5-yl)[2-(5-hydroxy-3-methylpyrazol-1-yl)-6-methyl-4-oxo-3,4-dihydropyrimidin-5-yl]phenylmethane

2-hydrazino-6-methylpyrimidin-4(3H)-one

ethyl acetoacetate

Downstream raw materials:

(2,4,6-trioxo-1,2,3,4,5,6-hexahydropyrimidin-5-yl)[2-(5-hydroxy-3-methylpyrazol-1-yl)-6-methyl-4-oxo-3,4-dihydropyrimidin-5-yl]phenylmethane

C₁₉H₂₁N₅O₂

C₁₇H₁₆BrN₅O₂

C₁₇H₁₇N₅O₂

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