dimethyl 3-[3-(4-octadecanoylaminophenyl)propionylamino]-3',4-oxydibenzoate

Base Information

Chemical Name:dimethyl 3-[3-(4-octadecanoylaminophenyl)propionylamino]-3',4-oxydibenzoate
CAS No.:227275-14-1
Molecular Formula:C₄₃H₅₈N₂O₇
Molecular Weight:714.943
Hs Code.:

Synonyms:dimethyl 3-[3-(4-octadecanoylaminophenyl)propionylamino]-3',4-oxydibenzoate

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Chemical Property of dimethyl 3-[3-(4-octadecanoylaminophenyl)propionylamino]-3',4-oxydibenzoate

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Technology Process of dimethyl 3-[3-(4-octadecanoylaminophenyl)propionylamino]-3',4-oxydibenzoate

There total 9 articles about dimethyl 3-[3-(4-octadecanoylaminophenyl)propionylamino]-3',4-oxydibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.4%

: 112-76-5
Stearoyl chloride

: 227275-26-5
dimethyl 3-[3-(4-aminophenyl)propionylamino]-3',4-oxydibenzoate

: 227275-14-1
dimethyl 3-[3-(4-octadecanoylaminophenyl)propionylamino]-3',4-oxydibenzoate

Guidance literature:: With triethylamine; In chloroform; at 20 ℃; for 21h;
DOI:10.1016/S0968-0896(01)00023-2

Reference yield:

: 19438-10-9
methyl 3-hydroxybenzoate

: 227275-14-1
dimethyl 3-[3-(4-octadecanoylaminophenyl)propionylamino]-3',4-oxydibenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 91.8 percent / K₂CO₃ / dimethylformamide / 6 h / 20 °C

2: H₂ / Pd/C / methanol; dioxane / 1 h / 20 °C / 2280 Torr

3: 72.4 percent / Et₃N / CHCl₃ / 20 °C

4: H₂ / Pd/C / dioxane; methanol / 2 h / 20 °C

5: 68.4 percent / Et₃N / CHCl₃ / 21 h / 20 °C

With hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(01)00023-2

Reference yield:

: 329-59-9
4-fluoro-3-nitro-benzoic acid methyl ester

: 227275-14-1
dimethyl 3-[3-(4-octadecanoylaminophenyl)propionylamino]-3',4-oxydibenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 91.8 percent / K₂CO₃ / dimethylformamide / 6 h / 20 °C

2: H₂ / Pd/C / methanol; dioxane / 1 h / 20 °C / 2280 Torr

3: 72.4 percent / Et₃N / CHCl₃ / 20 °C

4: H₂ / Pd/C / dioxane; methanol / 2 h / 20 °C

5: 68.4 percent / Et₃N / CHCl₃ / 21 h / 20 °C

With hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(01)00023-2