1-(3-Aminopropoxy)-2,4-dichlorobenzene

Base Information

Chemical Name:1-(3-Aminopropoxy)-2,4-dichlorobenzene
CAS No.:50911-63-2
Molecular Formula:C₉H₁₁Cl₂NO
Molecular Weight:220.098
Hs Code.:
DSSTox Substance ID:DTXSID801286855

Synonyms:1-(3-aminopropoxy)-2,4-dichlorobenzene;50911-63-2;3-(2,4-dichlorophenoxy)propan-1-amine;SCHEMBL7536535;DTXSID801286855;AKOS000173091;3-(2,4-Dichlorophenoxy)-1-propanamine;EN300-59144;Z316909342

Suppliers and Price of 1-(3-Aminopropoxy)-2,4-dichlorobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-(3-Aminopropoxy)-2,4-dichlorobenzene

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:219.0217694
Heavy Atom Count:13
Complexity:146

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C=C1Cl)Cl)OCCCN

Technology Process of 1-(3-Aminopropoxy)-2,4-dichlorobenzene

There total 4 articles about 1-(3-Aminopropoxy)-2,4-dichlorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1251302-89-2
1-(3-azidopropoxy)-2,4-dichlorobenzene

: 50911-63-2
3-(2,4-dichlorophenoxy)propan-1-amine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 3h; Reflux; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.02.054

Reference yield:

: 6954-78-5
1-bromo-3-(2,4-dichlorophenoxy)propane

: 50911-63-2
3-(2,4-dichlorophenoxy)propan-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 85 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux; Inert atmosphere

With lithium aluminium tetrahydride; sodium azide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.02.054

Reference yield:

: 120-83-2,40477-79-0
2,4-dichlorophenol

: 50911-63-2
3-(2,4-dichlorophenoxy)propan-1-amine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 3 h / Reflux; Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 85 °C / Inert atmosphere

3: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux; Inert atmosphere

With lithium aluminium tetrahydride; sodium azide; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.ejmech.2011.02.054