Technology Process of C33H48N2O3Si
There total 9 articles about C33H48N2O3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethanol;
for 2.5h;
DOI:10.1021/ol0490633
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: t-BuOCl / CH2Cl2 / -78 °C
1.2: EtMgBr; i-PrOH / CH2Cl2 / 0 - 23 °C
2.1: imidazole / dimethylformamide
3.1: AcOH; H2O / tetrahydrofuran / 23 °C
4.1: PPh3; DEAD / tetrahydrofuran
5.1: 91 percent / Mo7O24(NH4)6*4H2O; aq. H2O2 / ethanol / 50 °C
6.1: 75 percent / KHMDS / tetrahydrofuran / 2 h / -78 - 20 °C
7.1: 96 percent / H2 / Pd/C / ethanol / 2.5 h
With
1H-imidazole; ammonium molybdate tetrahydrate; tert-butylhypochlorite; water; hydrogen; dihydrogen peroxide; potassium hexamethylsilazane; acetic acid; triphenylphosphine; diethylazodicarboxylate;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol0490633
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 75 percent / KHMDS / tetrahydrofuran / 2 h / -78 - 20 °C
2: 96 percent / H2 / Pd/C / ethanol / 2.5 h
With
hydrogen; potassium hexamethylsilazane;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol;
DOI:10.1021/ol0490633